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| GC-MS法测定干姜超临界CO2萃取物的化学成分及其姜酚类成分的追踪 | |
| 引用本文： | 史琪荣,王莉,闫荟,杨峰,陈艳,孙晓迪,孙世光. GC-MS法测定干姜超临界CO2萃取物的化学成分及其姜酚类成分的追踪[J]. 解放军药学学报, 2011, 27(4): 296-298,302. DOI: 10.3969/j.issn.1008-9926.2011.04.05 |
| 作者姓名： | 史琪荣 王莉 闫荟 杨峰 陈艳 孙晓迪 孙世光 |
| 作者单位： | 1. 北京军区总医院药剂科, 北京,100700 2. 北京军区总医院医保办公室, 北京,100700 3. 北京军区总医院药理科, 北京,100700 4. 北京军区总医院剂科, 北京,100700 |
| 摘 要： | 目的 分析干姜超临界CO2萃取物的化学成分,并追踪萃取物中的姜酚类成分.方法 采用超临界CO2萃取干姜药材,用气相色谱-质谱联用技术分析其成分,6-姜酚和1O-姜酚直接进样分析,将姜酚图谱与萃取物图谱进行对比分析.结果 从干姜超临界CO2萃取物中鉴定了52种成分.在6-姜酚和10-姜酚的气相色谱-质谱分析过程中追踪到两... |
| 关 键 词： | 干姜 超临界CO2 气相色谱-质谱 姜酚 |
Gas Chromatography-Mass Spectrometry Analysis of the CO_2 Supercritical Fluid Extract of Zingiber officinale Rosc.and Tracing of gingerol |
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| SHI Qi-rong,WANG Li,YAN Hui,YANG Feng,CHEN Yan,SUN Xiao-di,SUN Shi-guang. Gas Chromatography-Mass Spectrometry Analysis of the CO_2 Supercritical Fluid Extract of Zingiber officinale Rosc.and Tracing of gingerol[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2011, 27(4): 296-298,302. DOI: 10.3969/j.issn.1008-9926.2011.04.05 | |
| Authors: | SHI Qi-rong WANG Li YAN Hui YANG Feng CHEN Yan SUN Xiao-di SUN Shi-guang |
| Affiliation: | ①①Department of Pharmcy;②Medical Insurance Office;③Department of Pharmcology,General Hospital of Beijing Military Command,Beijing100700,China |
| Abstract: | Objective To analyze the CO2 supercritical fluid extract of Zingiber officinale Rosc.by gas chromatography-mass Spectrometry and trace the ginger constituents in the extract.Methods Zingiber officinale Rosc.was extacted by CO2 supercritical fluid technology and was analyzed by gas chromatography-mass spectrometry.6-gingerol and 10-gingerol were directly injected into gas chromatography-mass spectrometry.The chromatograms of the extract and gingerols were compared under the same condition.Results Fifty-two c... |
| Keywords: | Zingiber officinale Rosc. CO2 supercritical fluid extraction gas chromatography-mass spectrometry ginger |
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