| HPLC法测定扶正平消胶囊中吴茱萸次碱的含量研究 |
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| 引用本文： | 李盛建,钱跹,周瑾,吕磊,张国庆,赵亮. HPLC法测定扶正平消胶囊中吴茱萸次碱的含量研究[J]. 药学实践杂志, 2018, 36(3): 274-276 |
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| 作者姓名： | 李盛建 钱跹 周瑾 吕磊 张国庆 赵亮 |
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| 作者单位： | 上海东方肝胆外科医院药材科, 上海 200438,上海东方肝胆外科医院药材科, 上海 200438,上海东方肝胆外科医院药材科, 上海 200438,上海东方肝胆外科医院药材科, 上海 200438,上海东方肝胆外科医院药材科, 上海 200438,上海东方肝胆外科医院药材科, 上海 200438 |
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| 摘 要： | 目的 建立高效液相色谱法测定扶正平消胶囊中吴茱萸次碱含量的方法。方法 样品经乙醇提取，乙酸乙酯液-液萃取后测定，色谱柱为Agilent TC-C18，流动相为乙腈-四氢呋喃甲酸水溶液（2%四氢呋喃+0.2%甲酸），流速为1.0 ml/min，柱温为40℃，检测波长为240 nm。结果 吴茱萸次碱含量在1.18~118 μg/ml范围内线性关系良好，r=0.999 9；其中日内、日间精密度RSD均<2%，平均加样回收率为94.20%。结论 本法准确、专属性强、重复性好，可用于测定扶正平消胶囊中吴茱萸次碱的含量。
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| 关 键 词： | 高效液相色谱 吴茱萸次碱 扶正平消胶囊 质量标准 |
| 收稿时间： | 2017-05-24 |
| 修稿时间： | 2018-03-12 |
Determination of rutaecarpine in Fuzhengpingxiao capsule by HPLC method |
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| LI Shengjian,QIAN Xian,ZHOU Jin,L,#; Lei,ZHANG Guoqing and ZHAO Liang. Determination of rutaecarpine in Fuzhengpingxiao capsule by HPLC method[J]. The Journal of Pharmaceutical Practice, 2018, 36(3): 274-276 |
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| Authors: | LI Shengjian,QIAN Xian,ZHOU Jin,L&# Lei,ZHANG Guoqing ZHAO Liang |
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| Affiliation: | Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China,Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China,Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China,Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China,Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China and Department of Pharmacy, Shanghai Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China |
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| Abstract: | |
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| Keywords: | HPLC rutaecarpine Fuzhengpingxiao capsule quality standard |
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