| 椿乳凝胶质量控制方法研究 |
| |
| 引用本文： | 张杰,龚云,向大雄,罗杰英,周春山.椿乳凝胶质量控制方法研究[J].北京中医药大学学报,2006,29(2):122-124,127. |
| |
| 作者姓名： | 张杰 龚云 向大雄 罗杰英 周春山 |
| |
| 作者单位： | 中南大学湘雅三医院,湖南,410013;株洲千金药业股份有限公司,湖南,412003;中南大学湘雅二医院临床药学研究室,湖南,410011;湖南中医学院药学院,湖南,410007;中南大学化学化工学院,湖南,410083 |
| |
| 摘 要： | 目的制定椿乳凝胶质量标准。方法采用薄层色谱法(TLC)鉴别牡丹皮和冰片,高效液相色谱法(HPLC)测定苦参碱的含量。结果薄层斑点清晰,重现性好;椿乳凝胶中苦参碱平均加样回收率为97.94%,RSD为3.16%。结论本法简便、准确,可有效控制椿乳凝胶质量。
|
| 关 键 词： | 椿乳凝胶 苦参碱 高效液相色谱 丹皮酚 冰片 薄层色谱 |
| 修稿时间： | 2005年4月11日 |
Quality control standard for Chunru gel |
| |
| ZHANG Jie,GONG Yun,XIANG Da-xiong,LUO Jie-ying,ZHOU Chun-shan.Quality control standard for Chunru gel[J].Journal of Beijing University of Traditional Chinese Medicine,2006,29(2):122-124,127. |
| |
| Authors: | ZHANG Jie GONG Yun XIANG Da-xiong LUO Jie-ying ZHOU Chun-shan |
| |
| Abstract: | Objective To set down the quality control standard for Chunru gel.Methods Cortex Moutan and Borneolum syntheticum were identified by thin layer chromatography(TLC),and the content of matrine was determined by HPLC.Result The result showed that the spots of TLC were fairly clear,the repeatability was good and the average sample-adding recovery of matrine was 97.94%(RSD=3.16%).Conclusion The method is simple,accurate and qualified for the quality control of Chunru gel effectively. |
| |
| Keywords: | Chunru gel matrine HPLC paeonolum borneolum syntheticum thin layer chromatography |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
