| 裸花紫珠的研究进展 |
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| 引用本文： | 蔡金平,董 琳,关薇薇,刘明生.裸花紫珠的研究进展[J].医学教育探索,2012,27(1):60-64. |
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| 作者姓名： | 蔡金平 董 琳 关薇薇 刘明生 |
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| 作者单位： | 山西中医学院，山西 太原 030024;黑龙江中医药大学，黑龙江 哈尔滨 150040;山西中医学院，山西 太原 030024 |
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| 基金项目： | 国家科技部“973”计划项目（2010CB735604） |
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| 摘 要： | 目的 建立复方洋参归地丸的质量标准。方法 采用薄层色谱法对制剂中当归、川芎、何首乌、石菖蒲、黄芪进行定性鉴别；采用高效液相色谱–蒸发光散射（HPLC-ELSD）法测定人参皂苷Rb1。结果 薄层色谱鉴别的色谱斑点清晰，阴性对照无干扰。人参皂苷Rb1在1.832～18.320 μg呈良好的线性关系，平均回收率为100.06%，RSD为1.69%（n=6）。结论 所建立的方法简便可行，专属性强，重现性好，可用于复方洋参归地丸的质量控制。
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| 关 键 词： | 复方洋参归地丸 当归 川芎 何首乌 石菖蒲 黄芪 薄层色谱 人参皂苷Rb1 高效液相色谱–蒸发光散射 |
Research progress of Callicarpa nudiflora |
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| CAI Jin-ping,DONG Lin,GUAN Wei-wei and LIU Ming-sheng.Research progress of Callicarpa nudiflora[J].Researches in Medical Education,2012,27(1):60-64. |
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| Authors: | CAI Jin-ping DONG Lin GUAN Wei-wei and LIU Ming-sheng |
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| Institution: | Shanxi College of Traditional Chinese Medicine, Taiyuan 030024, China;Heilongjiang University of Traditional Chinese Medicine, Harbin 150040, China;Shanxi College of Traditional Chinese Medicine, Taiyuan 030024, China |
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| Abstract: | Objective To optimize the sterilization technology of Ginseng Radix et Rhizoma with microwave. Methods The sterilization rate was used as the index to evaluate the technologies based on orthogonal test, in which the powder particle size of Ginseng Radix et Rhizoma, sterilization time, and microwave power were considered as three main technology factors, and the contents of ginsenosides were observed. Results The optimum condition was as follows: sterilization time 240 s, the powder particle size 10 mesh, and microwave power 6 000 W. Conclusion The new sterilization procedure is efficient and easy to operate. |
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| Keywords: | Compound Yangshen Guidi Pills Angelicae Sinensis Radix Chuanxiong Rhizoma Polygoni Multiflori Radix Acori Tatarinowii Rhizoma Astragali Radix TLC ginsenoside Rb1 HPLC-ELSD |
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