| HPLC法测定不同产地酸枣仁中酸枣仁皂苷A的含量 |
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| 引用本文： | 熊跃,曾文雪,何双凤.HPLC法测定不同产地酸枣仁中酸枣仁皂苷A的含量[J].江西中医学院学报,2013(6):56-57. |
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| 作者姓名： | 熊跃 曾文雪 何双凤 |
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| 作者单位： | [1]江西省南昌市中西医结合医院,南昌330003 [2]江西中医学院,南昌330006 [3]石家庄以岭药业股份有限公司,石家庄050035 |
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| 摘 要： | 目的：采用HPLC法测定不同产地酸枣仁中酸枣仁皂苷A的含量，并客观比较不同产地药材的质量。方法：用高效液相色谱法，使用Kromasil C18色谱柱（4．6mm×150mm，5μm）；流动相：乙腈-水（30：70），检测波长204nm，流速0．8mL/min，柱温25℃。结果：6个产地酸枣仁中酸枣仁皂苷A含量为0．5372％-0．0731％，不同产地酸枣仁中酸枣仁皂苷A含量有差异。结论：6个不同产地酸枣仁中酸枣仁皂苷A含量均符合药典标准，其中陕西延安产区的酸枣仁药材质量较其他产地相比较好。
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| 关 键 词： | 酸枣仁 酸枣仁皂苷A 高效液相色谱法 |
Determination of Jujubaside A in Different Origin Semen by HPLC |
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| Institution: | XIONG Yue , ZENG Wen - xue＊ , HE Shuang - feng( 1. Integrative Medicine Hospital of Nanchang , Jiangxi Nanehang 330003 ; 2. Jiangxi University of TCM, Nanchang 330006 ; 3. Shijiazhuang Yiling Pharmaceutial Co. Ltd, Shijiazhuang 050035) |
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| Abstract: | Objective： To develop a new method for the determination of Jujubaside A in different origin Semen. Methods：A HPLC method was set up , using Kromasil C18 column , Acetonitrile - water （30： 70） as the mobile phase with a flow rate 0.8 mL/min ,column temper ature 25℃. Results：The range of content of Jujubaside A in 6 origin Semen was 0. 5372% -0. 0731% . The content was difference . Conclusion ：Jujuboside A levels of Six different origin Semen were in line with pharmacopoeia standards . The Semen quality in Yanbaa was better than others. |
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| Keywords: | Semen Jujubaside A HPLC |
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