| 固相萃取结合高效液相色谱测定鸡肉中10种磺胺类药物残留 |
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| 引用本文： | 吴平谷,冯靓,王强,赵永信,谭莹,张晶,汤鋆,应英. 固相萃取结合高效液相色谱测定鸡肉中10种磺胺类药物残留[J]. 中国卫生检验杂志, 2008, 18(11) |
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| 作者姓名： | 吴平谷 冯靓 王强 赵永信 谭莹 张晶 汤鋆 应英 |
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| 作者单位： | 1. 浙江省疾病预防控制中心,杭州,310009
2. 浙江省农业科学院,杭州,310020 |
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| 基金项目： | 浙江省重点科研农业资助项目，浙江省重大科技攻关项目 |
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| 摘 要： | 目的:建立鸡肉中10种磺胺类药物残留的HPLC测定方法。方法:鸡肉经过甲醇提取,正己烷脱脂,SLW固相萃取柱净化,用HPLC法测定鸡肉中10种磺胺类药物的含量。结果:当鸡肉样品添加10种磺胺类药物为0.05~0.2 mg/kg时,方法回收率为67.4%~95.6%,变异系数为4.8%~11.5%,10种磺胺类药物最低检出浓度为0.01 mg/g。结论:以HPLC法测定鸡肉中10种磺胺类药物残留,操作简便、定量准确可靠。
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| 关 键 词： | 固相萃取 高效液相色谱 测定 磺胺 残留 |
Simultaneous determination of sulfonamide residues in chicken muscle by solid phase extraction and high performance liquid chromatography |
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| Wu Ping-gu,Fen Liang,Wang Qiang,Zhao Yong-xin,Tan Ying,Zhan Jing,Tan Jun,Ying Ying. Simultaneous determination of sulfonamide residues in chicken muscle by solid phase extraction and high performance liquid chromatography[J]. Chinses Journal of Health Laboratory Technology, 2008, 18(11) |
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| Authors: | Wu Ping-gu Fen Liang Wang Qiang Zhao Yong-xin Tan Ying Zhan Jing Tan Jun Ying Ying |
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| Affiliation: | Wu Ping-gu1,Fen Liang1,Wang Qiang2,Zhao Yong-xin1,Tan Ying1,Zhan Jing1,Tan Jun1,Ying Ying1 |
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| Abstract: | Objective:To establish an HPLC method for quantization of 10 sulfonamides residues in chicken muscle.Methods:Chicken muscle was extracted with methanol,defatted with n-hexane and cleaned up with SLW solid-phase extraction.Then the concentration of 10 sulfonamides residues was determined by HPLC.Results:The recoveries of 10 sulfonamides residues in chicken muscle were 67.4%~95.6%,with relative standard deviations between 4.8% and 11.5%.While the contents of added standard were 0.05~0.2 mg/kg.and the minimum detected limits of this method were 0.01 mg/kg.Conclusion:This is a simple,accurate and reliable method for determination of 10 sulfonamides residues in chicken muscle. |
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| Keywords: | Solid phase extraction HPLC Determination Sulfonamides Residue |
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