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运用GC-MS技术对2种淫羊藿挥发性成分的比较分析
引用本文:施启红,吕磊,李玲,赵亮,张国庆. 运用GC-MS技术对2种淫羊藿挥发性成分的比较分析[J]. 药学实践杂志, 2011, 29(6): 445-448
作者姓名:施启红  吕磊  李玲  赵亮  张国庆
作者单位:1. 启东市人民医院药材科,江苏启东,226200
2. 第二军医大学东方肝胆外科医院药材科,上海,200438
3. 第二军医大学药学院分析测试中心,上海,200433
摘    要:目的运用GC-MS技术对柔毛淫羊藿与朝鲜淫羊藿挥发性成分进行比较分析。方法采用水蒸气蒸馏法提取柔毛淫羊藿和朝鲜淫羊藿挥发油,运用气相色谱-质谱联用技术,结合计算机检索对其挥发油进行分离鉴定。结果共鉴定出2种淫羊藿中76个挥发性成分,其中28个共有成分。结论柔毛淫羊藿与朝鲜淫羊藿挥发油在组分和含量上存在一定的差异,本研究为2种淫羊藿药材的鉴别及质量控制提供了重要依据。

关 键 词:柔毛淫羊藿  朝鲜淫羊藿  挥发油  GC-MS
收稿时间:2011-06-25
修稿时间:2011-09-01

Analysis of the essential oil from two varieties of epimediums by GC-MS
SHI Qi-hong,LV Lei,LI Ling,ZHAO Liang and ZHANG Guo-qing. Analysis of the essential oil from two varieties of epimediums by GC-MS[J]. The Journal of Pharmaceutical Practice, 2011, 29(6): 445-448
Authors:SHI Qi-hong  LV Lei  LI Ling  ZHAO Liang  ZHANG Guo-qing
Affiliation:Department of Pharmacy, People's Hospital of Qidong, Qidong 200438, China;Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China;Pharmaceutical Analysis Center, School of Pharmacy, the Second Military Medical University of PLA, Shanghai 200433, China;Department of Pharmacy, People's Hospital of Qidong, Qidong 200438, China;Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China
Abstract:Objective To analyze the chemical components of the essential oil from Epimedium pubescens Maxim.and Epimedium koreanum Nakai. by GC-MS. Methods The essential oil was extracted from two epimediums by steam distillation, the chemical components of the essential oi1 were detected by GC-MS, peaks and their corresponding compounds were identified through database index. Results 76 chief components from two varieties of epimediums were identified, 24 components were noted in both. Conclusion There were some differences in composition and content between the two kinds of epimediums. A scientific basis for the further identification and quality control of the two different species of epimediums was offered in this paper.
Keywords:Epimedium pubescens Maxim  Epimedium koreanum Nakai  essential oil  GC-MS
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