| HPLC多波长法同时测定血府逐瘀颗粒中多指标成分的含量 |
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| 引用本文： | 刘征辉,叶挺祥,赵琳琳,程奕,罗国安. HPLC多波长法同时测定血府逐瘀颗粒中多指标成分的含量[J]. 中国中药杂志, 2010, 35(16): 2157-2160 |
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| 作者姓名： | 刘征辉 叶挺祥 赵琳琳 程奕 罗国安 |
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| 作者单位： | 1. 天津海世达检测技术有限公司,天津,300381;天津市现代中药质量检验中心,天津,300381
2. 清华大学,化学系,北京,100084 |
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| 基金项目： | 天津市科技发展计划项目(05SYSYGX25000);中药质量现状评价与标准研究 |
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| 摘 要： | 目的:研究建立血府逐瘀颗粒多指标成分同时定量的方法。方法:采用HPLC多波长法对苦杏仁苷、羟基红花黄色素A、芍药苷和阿魏酸进行含量测定。结果:结果表明苦杏仁苷进样量在0.115 4~0.923 2μg、羟基红花黄色素A进样量在0.021 9~0.175 4μg、芍药苷进样量在0.395 2~3.161 6μg、阿魏酸进样量在0.042 6~0.340 8μg与峰面积呈良好线性关系,平均回收率分别为101.78%,99.60%,98.90%,100.31%(RSD分别为1.7%,2.9%,2.0%,1.8%)。结论:所建立的定量方法快速简单,方法可靠,可作为血府逐瘀颗粒的质量控制方法。
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| 关 键 词： | 血府逐瘀颗粒 苦杏仁苷 羟基红花黄色素A 芍药苷 阿魏酸 HPLC |
| 收稿时间： | 2010-04-20 |
Simultaneous determination of multicomponent in Xuefuzhuyu granule with different UV-wavelength by HPLC |
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| LIU Zhenghui,YE Tingxiang,ZHAO Linlin,CHENG Yi and LUO Guoan. Simultaneous determination of multicomponent in Xuefuzhuyu granule with different UV-wavelength by HPLC[J]. China Journal of Chinese Materia Medica, 2010, 35(16): 2157-2160 |
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| Authors: | LIU Zhenghui YE Tingxiang ZHAO Linlin CHENG Yi LUO Guoan |
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| Affiliation: | Tianjin High-Standard Quality Testing Lab., Tianjin 300081, China;Tianjin Center for Quality Testing of Trditional Chinese Medicine, Tianjin 300081, China;Tianjin High-Standard Quality Testing Lab., Tianjin 300081, China;Tianjin Center for Quality Testing of Trditional Chinese Medicine, Tianjin 300081, China;Tianjin High-Standard Quality Testing Lab., Tianjin 300081, China;Tianjin Center for Quality Testing of Trditional Chinese Medicine, Tianjin 300081, China;Tianjin High-Standard Quality Testing Lab., Tianjin 300081, China;Tianjin Center for Quality Testing of Trditional Chinese Medicine, Tianjin 300081, China;Department of Chemistry, Tsinghua University, Beijing 100084, China |
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| Abstract: | |
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| Keywords: | Xuefuzhuyu granule Semen Armeniacae Amarum PE hydroxysafflor yellow A paeoniflorin ferulic acid HPLC |
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