| 静态顶空气相色谱-质谱联用鉴别硫黄熏制的柴胡 |
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| 引用本文： | 廖远熹,程志红,王昊阳,郭寅龙,邵应男.静态顶空气相色谱-质谱联用鉴别硫黄熏制的柴胡[J].中国中药杂志,2005,30(24):1909-1911. |
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| 作者姓名： | 廖远熹 程志红 王昊阳 郭寅龙 邵应男 |
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| 作者单位： | 1. 中国科学院,上海有机化学研究所,上海,200032
2. 洛阳民生药业有限责任公司,河南,洛阳,471002 |
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| 摘 要： | 目的:鉴别市售柴胡是否用硫黄熏制。方法:运用静态顶空毛细管气相色谱-质谱联用技术进行检测市售柴胡是否经硫黄熏蒸,并从产地采集未经硫黄熏蒸的柴胡作为阴性对照药材与市售柴胡进行比较。结果:阴性与阳性药材差异显著,考察了9种不同产地的市售柴胡,其中的6种柴胡检出硫黄。结论:本方法可用于快速鉴别市售柴胡是否经硫黄熏制。
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| 关 键 词： | 柴胡 硫黄 静态顶空-气相色谱-质谱联用 |
| 文章编号： | 1001-5302（2005）24-1909-03 |
| 收稿时间： | 2004-05-15 |
| 修稿时间： | 2004-05-15 |
Identification of the fumatory Radix Bupleuri with sulfur by static headspace GC-MS |
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| LIAO Yuan-xi;CHENG Zhi-hong;WANG Hao-yang;GUO Yin-long;SHAO Ying-nan.Identification of the fumatory Radix Bupleuri with sulfur by static headspace GC-MS[J].China Journal of Chinese Materia Medica,2005,30(24):1909-1911. |
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| Authors: | LIAO Yuan-xi;CHENG Zhi-hong;WANG Hao-yang;GUO Yin-long;SHAO Ying-nan |
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| Institution: | 1. Chinese Academy of Sciences, Shanghai Institute of Organic Chemistry, Shanghai 200032, China ; 2. Luoyang Minsheng Pharmaceutical Co.,Luoyang 471002, China |
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| Abstract: | Objective: To identify whether Radix Bupleuri(Bupleurum chinense) was fumed with sulfur.Method: A static headspace GC-MS method was used to detect sulfur in the fumatory Radix Bupleuri,the authentic samples free of sulfur was detected as reference.Result: Sulfur was detected in six samples from nine samples collected in different locations.Conclusion: The method can be used to detect sulfur rapidly in the fumatory Radix Bupleuri with sulfur. |
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| Keywords: | Bupleurum chinense sulfur static headspace GC-MS |
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