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薤白微量元素的测定
引用本文:吴素珍,李加林,李银保.薤白微量元素的测定[J].时珍国医国药,2007,18(11):2654-2655.
作者姓名:吴素珍  李加林  李银保
作者单位:赣南医学院,江西,赣州,341000
基金项目:赣南医学院人才引进科研资助项目(No2006064)
摘    要:目的运用火焰原子吸收光谱法测定薤白中Fe,Cu,Zn,Mn,Ca,Mg6种微量元素的含量。方法用浓硝酸微波消解样品,采用标准曲线法测定。结果所测定的薤白中含有丰富的人体必需微量元素,采用此方法回收率在95.00%~102.80%之间,相对标准偏差(RSD)小于2.8214%。结论该方法简单、准确,结果令人满意。

关 键 词:微波消解  火焰原子吸收光谱法  微量元素  薤白
文章编号:1008-0805(2007)11-2654-01
收稿时间:2007-03-13
修稿时间:2007-05-17

Determination of the Trace Elements in Allium macrostemon
WU Su-zhen,LI Jia-lin,LI Yin-bao.Determination of the Trace Elements in Allium macrostemon[J].Lishizhen Medicine and Materia Medica Research,2007,18(11):2654-2655.
Authors:WU Su-zhen  LI Jia-lin  LI Yin-bao
Institution:Department of Biochemistry and Molecular Biology, Gannan Medical University, Ganzhou, Jiangxi 341000, China
Abstract:Objective To determine the contents of six trace elements by flame atomic absorption spectroscopy including Fe,Cu,Zn,Mn,Ca,Mg in bulb and root of Allium macrostemon. Methods The sample was diluted by microwave with HNO3, and the contents were determined by calibration curve method. Results The results showed that the Allium macrostemon contains rich trace elements which is necessary for people. The recovery was in the range of 95.00%~102.80% and the RSD was less than 2.821 4%.Conclusion The method is simple, accuarate and satisfactory.
Keywords:Microwave digestion  Flame atomic absorption spectrometry  Trace elements  Allium macrostemon
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