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| 气相色谱法测定行军散中丁香酚的含量 | |
| 引用本文： | 王喆桅,金城,焦懿,王伽伯,朱珊薇,谭睿,肖小河.气相色谱法测定行军散中丁香酚的含量[J].解放军药学学报,2010,26(2):137-138. |
| 作者姓名： | 王喆桅 金城 焦懿 王伽伯 朱珊薇 谭睿 肖小河 |
| 作者单位： | 1. 100039,北京,解放军302医院中药研究所;610031,四川成都,西南交通大学生命科学与工程学院 2. 解放军302医院中药研究所,北京,100039 3. 100039,北京,解放军302医院中药研究所;410007,湖南长沙,湖南中医药大学药学院 4. 西南交通大学生命科学与工程学院,四川成都,610031 |
| 基金项目： | 重大新药创制专项,No.2009ZXJ09004-057 |
| 摘 要： | 目的建立行军散中丁香酚的含量测定方法。方法色谱柱为HP-5（25m×0.32mm×0.52μm）;固定相为5%苯基甲基聚硅氧烷;FID检测器;进样口温度240℃;起始柱温110℃;程序升温;载气为氩气。结果在该色谱条件下,提取物挥发油中丁香酚的含量在65.9～395.4μg范围内呈良好线性关系（r2=0.9991）。结论该方法具有便捷、准确、重复性高等优点,可以作为行军散中丁香酚含量的测定方法。 |
| 关 键 词： | 行军散 丁香酚 气相色谱法 |
Assaying of Eugenol in Xingjunsan by Gas Chromatography Method |
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| WANG Zhe-wei,JIN Cheng,JIAO Yi,WANG Jia-bo,ZHU Shan-wei,TAN Rui,XIAO Xiao-he.Assaying of Eugenol in Xingjunsan by Gas Chromatography Method[J].Pharmaceutical Journal of Chinese People's Liberation Army,2010,26(2):137-138. | |
| Authors: | WANG Zhe-wei JIN Cheng JIAO Yi WANG Jia-bo ZHU Shan-wei TAN Rui XIAO Xiao-he |
| Institution: | (①PLA Institute of Chinese Materia Medica,Hospital 302 of PLA, Beijing 100039,China;②School of Life Science and Engineering, Southwest Jiaotong University, Chengdu 610031,China;③College of Pharmaceutical Sciences, Hunan University of Chinese Medicine, Changsha 410007,China) |
| Abstract: | Objective To determine the content of eugenol in Xingjunsan by gas chromatography Method. Methods The gas chromatography colum was HP-5 （25 m×0.32 mm×0.52 μm）,and the static phase was 5% phenylmethylpolysiloxane.With the FID detector, the temperature of sample injection was 240℃ while the initiation temperature was 110 ℃.The programmed heating method was used with argon as carrier gas. Results The linearity of eugenol content was good within the range of 65.9-395.4 μg（r2=0.9991）. Conclusion This method is simple, accurate and reproducible, and can be used for assaying of eugenol in Xingjunsan. |
| Keywords: | Xingjunsan eugenol gas chromatography method |
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