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四磨汤挥发油化学成分GC/MS联用对比分析
引用本文:马丽,郭建生,曾贵荣.四磨汤挥发油化学成分GC/MS联用对比分析[J].中医药导报,2013(11):73-75.
作者姓名:马丽  郭建生  曾贵荣
作者单位:湖南中医药大学,湖南省中药现代化重点实验室,湖南长沙410208
基金项目:湖南省研究生创新项目(02410901002003)
摘    要:目的:分析四磨汤挥发油化学成分。方法:采用水蒸汽蒸馏法提取四磨汤挥发油,经(Gc/Ms)计算机联用技术分离鉴定。结果:从四磨汤挥发油中分离出67个峰,鉴定了其中29种化学成分,占挥发油总量的61.27%。四磨汤挥发油主要成分:马兜铃烯(9.86%),2,4-二异丙1-甲1-乙烯基环己烷(6.29%),肉豆蔻酸(5.92%),3-乙基-3-羟基雄甾烷基-17-酮(5.9%),棕榈酸(4.17%)等。结论:为进一步研究四磨汤复方的物质基础提供了科学依据。

关 键 词:四磨汤  挥发油  化学成分  气相色谱  质谱联用分析

Analysis on Volatile Components in Simo Decoction with GC-MS
MA Li,GUO Jian-sheng,ZENG Gui-rong.Analysis on Volatile Components in Simo Decoction with GC-MS[J].GUIDING JOURNAL OF TCM,2013(11):73-75.
Authors:MA Li  GUO Jian-sheng  ZENG Gui-rong
Institution:(Hunan University of Chinese Medicine, Key Laboratory of Traditional Chinese Medicine Modernization Changsha Hunan 410208, China)
Abstract:Objective: To analyze the main constituents of yohile oil from Simo Decoction. Methods: Volatile oil was obtained by steam distillation technique. The chemical constituents were separated and indentified by GC/MS. Results: There were 67 peaks shown from the volatile oil, from which, 29 chemical constituents were identified, which accounting for 61.27% of the volatile oil. The main constituents in volatile oil are Aristolene(9.86%), 2, 4-Diisopropenyl-l-methyl-l-vinylcyclohexane (6.29%), myristic acid(5.92%), 3-ethyl-3-hydroxy androsterone alkyl-17-ketone(5.9%) and cetylic acid(4.17%). Conclusion: This research provides the basis for the further study of active components from Simo Decoction.
Keywords:Simo Decoction  Volatile oil  Chemical composition  GC-MS
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