| HPLC法测定枳壳饮片中辛弗林的含量 |
| |
| 引用本文： | 蒋以号,曹旻旻,龚千锋.HPLC法测定枳壳饮片中辛弗林的含量[J].中华中医药杂志,2011(10):2363-2364. |
| |
| 作者姓名： | 蒋以号 曹旻旻 龚千锋 |
| |
| 作者单位： | 南昌大学环境与化学工程学院;康美药业股份有限公司;江西中医学院; |
| |
| 基金项目： | 江西省科技厅重大项目(赣科发计字[2007]189号)~~ |
| |
| 摘 要： | 目的:对枳壳生品及不同炮制品中辛弗林的含量进行考察。方法:色谱柱为E1823028 C18柱(250mm×4.6mm,5μm);流动相:甲醇-0.01mol/L盐酸(52:48),柱温30℃,流速1.0mL/min,检测波长285nm。结果:樟帮炮制品中的辛弗林含量低于药典法炮制品。结论:枳壳不同炮制品的内在质量有明显差异。
|
| 关 键 词： | 枳壳 辛弗林 含量测定 高效液相色谱 |
Determination of synephrine in Fructus Aurantii and its processed products by HPLC |
| |
| JIANG Yi-hao,CAO Min-min,GONG Qian-feng.Determination of synephrine in Fructus Aurantii and its processed products by HPLC[J].China Journal of Traditional Chinese Medicine and Pharmacy,2011(10):2363-2364. |
| |
| Authors: | JIANG Yi-hao CAO Min-min GONG Qian-feng |
| |
| Institution: | JIANG Yi-hao1,CAO Min-min2,GONG Qian-feng3(1College of Environmental and Chemical Engineering,Nanchang University,Nanchang 330031,China,2Kangmei Pharmaceutical Limited Company,Puning 515341,3Jiangxi College of TCM,Nanchang 330004,China) |
| |
| Abstract: | Objective: To explore the contents of synephrine in Fructus Aurantii and its processed products.Methods: The chromatographic conditions were as follows: E1823028 C18 Column(250mm×4.6mm,5μm),mobile phase of methanol-0.01%chlorhydric acid(volume ratio of 52:48),the column temperature at 30℃,flow phase rate being 1.0mL/min and detection wavelength at 285nm.Results: Synephrine contents of the product processed by Zhang-Bang method were lower than that of by Pharmacopoeia method.Conclusion: There is a significant difference in intrinsic quality among various processed products of Fructus Aurantii. |
| |
| Keywords: | Fructus Aurantii Synephrine Content determination HPLC |
| 本文献已被 CNKI 等数据库收录！ |
|
