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通脉降脂胶囊中姜黄素、游离大黄酸及大黄素含量的测定
引用本文:韩刚,喇万英,赵琳琳,邢晓琴. 通脉降脂胶囊中姜黄素、游离大黄酸及大黄素含量的测定[J]. 华北煤炭医学院学报, 2004, 6(4): 416-417
作者姓名:韩刚  喇万英  赵琳琳  邢晓琴
作者单位:1. 华北煤炭医学院药学系,河北唐山,063000
2. 华北煤炭医学院中医系,河北唐山,063000
摘    要:①目的测定通脉降脂胶囊中姜黄素、游离大黄酸、游离大黄素的含量。②方法采用薄层层析-比色的方法测定通脉降脂胶囊中各成分的含量。③结果每粒胶囊中各成平均含量分别为姜黄素3.04mg、游离大黄酸0.144mg、游离大黄素0.227mg。RSD分别为2.7%、0.85%、2.0%。回收率分别为98.7%、102.3%、98、3%。④结论薄层层析一比色法测定通脉降脂胶囊中的主要成分方法回收率较好,比较适合医院药房及中小企业对中药制剂的质量控制。

关 键 词:通脉降脂胶囊 姜黄素 大黄酸 大黄素
文章编号:1008-6633(2004)04-0416-02
修稿时间:2004-04-16

Detactian of the contents of curcumin, free rhein and free emodin in Tongmaijiangzhi capsule
HAN Gang,LA Wanying,ZHAO Linlin,et al.. Detactian of the contents of curcumin, free rhein and free emodin in Tongmaijiangzhi capsule[J]. Journal of North China Coal Medical College, 2004, 6(4): 416-417
Authors:HAN Gang  LA Wanying  ZHAO Linlin  et al.
Abstract:Objective To determine the contents of curcumin, free rhein and free emodin in Tongmaijiangzhi Capsule.Methods The contents of curcumin, free Rhein and free Emodin in Tongmaijiangzhi Capsule were detacted by useing TLC-Colorimetric method. Results The average contents for curcumin, free rehin and free cmodin are 3.04 mg,0.144 mg, 0.227 mg respectively, and the relative standard deviation (RSD) are 2.7%, 0.85%, 2.0% respectively,rate of recovery are 98.7%, 102.3%, 98.3% in every capsule. Conclusion TLC-Colorimetric method to determine the main contents in Tongmaijiangzhi Capsule is better for its rate of recovery. It is suitable for pharmacy in hospital or small enterprise to control the Chinese Tradition Medicine quality.
Keywords:Tongmaijiangzhi capsule  Curcuma  Rhein  Emodin
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