| 水中微量毒鼠强的GC/MS/MS测定法 |
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| 引用本文： | 符展明,金永高,杨勇,符超. 水中微量毒鼠强的GC/MS/MS测定法[J]. 中国卫生检验杂志, 2005, 15(3): 302-303 |
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| 作者姓名： | 符展明 金永高 杨勇 符超 |
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| 作者单位： | 1. 宁波市疾病预防控制中心,浙江宁波,315010
2. 宁波市自来水公司,浙江宁波,315040 |
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| 摘 要： | 目的：本文研究应用GC／MS／MS法(气相色谱／质谱检测法)测定水中微量毒鼠强。方法：用苯萃取，过无水硫酸钠柱脱水、活性炭脱色净化。GC／MS／MS法测定。结果：本方法的精密度变异系数(CV)为3．9％～5．4％，平均回收率为92．0％～94．8％，最低检测限为1．0ng／L。结论：本法操作方便、灵敏度高、准确性好，不但能快速准确检定水中微量毒鼠强的要求，而且能满足中毒患者血液、尿液、胃液样品中的痕量毒鼠强。
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| 关 键 词： | 毒鼠强 GC／MS／MS法 中毒患者 胃液 尿液 血液 研究应用 微量 无水硫酸钠 测定法 |
| 文章编号： | 1004-8685(2005)03-0302-02 |
| 修稿时间： | 2004-11-25 |
Study on the determination of tetrame thylendisulfotetramin in water by GC/MS/MS |
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| FU Zhan-ming,Jin Yong-gao,Yang Yong,FU Chao. Study on the determination of tetrame thylendisulfotetramin in water by GC/MS/MS[J]. Chinses Journal of Health Laboratory Technology, 2005, 15(3): 302-303 |
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| Authors: | FU Zhan-ming Jin Yong-gao Yang Yong FU Chao |
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| Affiliation: | Fu Zhan-ming1,Jin Yong-gao1,Yang Yong2,Fu Chao2 |
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| Abstract: | Objective:To study the method and condition for detection of tetrame thylendisulfotetramin in water by GC/MS/MS.Methods:All samples were purified by benzene,anhydrous sodium sulfate,active carbon,and then analyzed by GC/MS/MS.Results:The detection limit was 1.0 pg/kg,coefficient of variation was 3.9%~5.4%,the rate of recovery was 9.2%~94.8%.Conclusion:The method was sensitive,selective,repeatable and accurate. [ |
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| Keywords: | Water Tetrame thylendisulfotetramin GC/MS/MS |
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