| 补血益母颗粒质量标准研究 |
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| 引用本文： | 邝薛洪,谭伯森,陈敏坚. 补血益母颗粒质量标准研究[J]. 现代医药卫生, 2014, 0(6): 24-26 |
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| 作者姓名： | 邝薛洪 谭伯森 陈敏坚 |
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| 作者单位： | [1]广州市荔湾区第二人民医院,广东广州510160 [2]广州医学院荔湾医院,广东广州510170 |
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| 摘 要： | 目的研究补血益母颗粒中阿胶及黄芪的测定方法，为建立其质量标准提供数据依据。方法采用薄层色谱鉴别颗粒中的阿胶及黄芪，并以高效液相色谱法（HPLC）测定黄芪甲苷的含量。结果在薄层色谱中能清晰鉴别出阿胶及黄芪，HPLC法测定黄芪甲苷在1．01-50．10μg时线性关系良好（R2=O．9999）。结论薄层色谱法鉴别补血益母颗粒中阿胶及黄芪以及HPLC法测定黄芪甲苷的含量，方法简便准确，重现性好，专属性强，可作为补血益母颗粒的质量控制方法。
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| 关 键 词： | 色谱法，薄层 方法 色谱法，高压液相 方法 阿胶 补血益母颗粒 黄芪甲苷 质量标准 |
Studies on quality standard of Buxue Yimu Granule |
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| Kuang Xuehong,Tan Bosen,Chen Minjian. Studies on quality standard of Buxue Yimu Granule[J]. JOURNAL OF MODERN MEDICINE & HEALTH, 2014, 0(6): 24-26 |
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| Authors: | Kuang Xuehong Tan Bosen Chen Minjian |
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| Affiliation: | 1. Guangzhou Municipal Liwan District Second People＇s Hospital, Guangzhou, Guangdong 510160, China; 2. Liwan Hospital of Guangzhou Medical Col- lege, Guangzhou , Guangdong 510170, China) |
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| Abstract: | Objective To study the assay method of Colla Corii Asini and Angelicae Sinensis in Buxue Yimu Granule,in order to provide basis for establishing quality standard. Methods The thin layer chromatography （TLC） was applied for distin- guishing Colla Corii Asini and Angelicae in Buxue Yimu Granule, while high performance liquid chromatography （HPLC） was used for the content determination of astragaloside. Results Colla Corii Asini and Angelicae Sinensis could be identified by TLC, and astragaloside showed good linear relation during 1.01-50.10 p~g （R~0.999 9） by HPLC. Conclusion The TLC for iden- tification of Colla Corii Asini and Angelicae Sinensis in Buxue Yimu Granule, and HPLC for determination the content of ostraga- loside are simple,accurate ,reliable and reproducible with strong specificity,which can be used as quality control standard of Buxue Yimu Granule. |
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| Keywords: | Chromatography,thin layer/methods Chromatography,high pressure liquid/methods Colla corii asini Buxue yimu granule Astragaloside Quality standard |
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