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飞龙掌血石油醚部位的化学成分研究
引用本文:石磊,王微,姬志强,康文艺. 飞龙掌血石油醚部位的化学成分研究[J]. 中国药房, 2012, 0(27): 2531-2532
作者姓名:石磊  王微  姬志强  康文艺
作者单位:[1]解放军第155中心医院,河南开封475003 [2]河南大学中药研究所,河南开封475004
基金项目:解放军济南军区后勤科研计划项目(CYNl0L067)
摘    要:目的:研究飞龙掌血石油醚部位的化学成分。方法:采用薄层色谱、硅胶与凝胶柱色谱法对飞龙掌血石油醚部位进行分离纯化,通过理化方法和波谱数据进行结构鉴定。结果:从飞龙掌血的石油醚部位中分离得到6个化合物,通过波谱数据及理化性质分别鉴定为十八酸(1)、油酸(2)、亚油酸(3)、β-谷甾醇(4)、茴芹内酯(5)和去甲白屈菜红碱(6)。其中化合物1~3为首次从该植物中分离得到。结论:本试验结果可为飞龙掌血的进一步研究提供依据。

关 键 词:飞龙掌血  石油醚部位  化学成分  十八酸  油酸  亚油酸

Study on Chemical Constituents in Petroleum Parts of Toddafia asiatica
SHI Lei,JI Zhi-qiangNo.,Central Hospital of PLA,Henan Kaifeng,China WANG Wei,KANG Wen-yi. Study on Chemical Constituents in Petroleum Parts of Toddafia asiatica[J]. China Pharmacy, 2012, 0(27): 2531-2532
Authors:SHI Lei  JI Zhi-qiangNo.  Central Hospital of PLA  Henan Kaifeng  China WANG Wei  KANG Wen-yi
Affiliation:(Institute of Chinese Materia Medica, Henan University, Henan Kaifeng 475004, China)
Abstract:OBJECTIVE: To study the chemical constituents in petroleum parts of Toddalia asiatica. METHODS: The com- pounds were isolated from petroleum parts of T. asiatica and purified by TLC, silica gel and gel column chromatography. The struc- tures were elucidated by physicochemical properties and spectral analysis. RESULTS: Six compounds were obtained and elucidated as octadecanoic acid (1), oleic acid (2), linoleic acid (3), fl-sitosterol (4), pimpinellin (5) and norchelerythrine (6) by physico- chemical properties and spectral analysis. Compounds 1~3 were isolated from the plant for the first time. CONCLUSION: The tri- al results provide reference for further study of T. asiatica.
Keywords:Toddalia asiatica  Petroleum part  Chemical components  Octadecanoic acid  Oleic acid  Linoleic acid
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