| 益肾颗粒中有机氯农药残留量检测 |
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| 引用本文： | 刘雅琴,薛坤.益肾颗粒中有机氯农药残留量检测[J].中国药房,2012(27):2563-2565. |
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| 作者姓名： | 刘雅琴 薛坤 |
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| 作者单位： | 天津中医药大学第一附属医院,天津300193 |
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| 摘 要： | 目的:考察益肾颗粒中有机氯农药残留情况。方法:采用丙酮-水提取系统、二氯甲烷液分配、浓硫酸磺化净化技术制备供试品溶液,以毛细管气相色谱法检测益肾颗粒中9种有机氯农药残留量;色谱柱为弹性石英毛细管SE-54(30m×0.32mm×0.25μm),进样口温度为230℃,检测器温度为300℃。结果:9种有机氯农药的最低检测限范围为0.128～0.446ng·g-1,平均加样回收率范围为72.64%～114.77%(n=9)。结论:所检测的10批益肾颗粒中有机氯农药残留量均符合国家相关标准。
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| 关 键 词： | 毛细管气相色谱法 有机氯农药残留 益肾颗粒 |
Determination of Residual Organic Chlorine Pesticide in Yishen Granules |
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| LIU Ya-qin,XUE Kun.Determination of Residual Organic Chlorine Pesticide in Yishen Granules[J].China Pharmacy,2012(27):2563-2565. |
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| Authors: | LIU Ya-qin XUE Kun |
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| Institution: | (The First Affiliated Hospital of Tianjin University of TCM,Tianjin 300193, China) |
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| Abstract: | OBJECTIVE： To investigate the residual organic chlorine pesticide in Yishen granules, METHODS： Acetone-water extraction system, methylene chloride fluid-fluid assignment and strong sulfuric acid sulfonation purification technology were used to prepare test sample solution. The quantities of 9 kinds of residual organic chlorine pesticide were determined by capillary GC. Elastic quartz capillary vessel SE-54 column（30 mx0.32 mm×0.25μm） was used, the injector temperature 230℃ and the detec- tor temperature was 300 ℃. RESULTS： The lowest examination limits of 9 kinds of residual organic chlorine pesticide were 0.128-0.446 ng·g-1, and average recovery tests were 72.64%-114.77% （n=9）. CONCLUSION： The quantity of organic chlo- rine pesticide residues in 10 batches of Yishen granules conforms to the related national standard. |
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| Keywords: | Capillary GC Organic pesticide residues Yishen granules |
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