| 乳欣安胶囊质量标准研究 |
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| 引用本文： | 范永春. 乳欣安胶囊质量标准研究[J]. 中成药, 2010, 32(5) |
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| 作者姓名： | 范永春 |
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| 作者单位： | 江苏省中医药研究院,江苏,南京,210028 |
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| 摘 要： | 目的:研究乳欣安胶囊(淫羊藿、蛇床子、全蝎)中活性物质淫羊藿苷、蛇床子素的测定及蛇床子、全蝎鉴定。方法:采用薄层色谱法对该复方中蛇床子、全蝎药材进行色谱鉴别,HPLC法测定乳欣安胶囊中淫羊藿苷和蛇床子素的含量。结果:该制剂中,蛇床子、全蝎有良好的展开系统,不存在阴性干扰。淫羊藿苷在61.7ng～740.4ng范围内呈良好的线性关系,r=0.9996,平均回收率为99.86%,RSD为0.82%;蛇床子素在57.4ng～688.8ng范围内有良好的线性关系,r=0.9998,平均回收率为99.55%,RSD为0.71%。结论:本方法简便可行,可做为乳欣安胶囊的质量标准。
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| 关 键 词： | 乳欣安胶囊 淫羊藿苷 蛇床子素 薄层色谱 高效液相色谱 |
Quality standard for Ruxinan Capsule |
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| FAN Yong-chun. Quality standard for Ruxinan Capsule[J]. Chinese Traditional Patent Medicine, 2010, 32(5) |
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| Authors: | FAN Yong-chun |
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| Affiliation: | FAN Yong-chun (Jiangsu Provincial Institute of Traditional Chinese Medicine,Nanjing 210028,Jiangsu,China) |
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| Abstract: | AIM: To determine quantitatively active ingredients,icariine and osthole,and to identify Fructus Cnidium and Scorpio in Ruxinan Capsule ( Folium Epimedii,Fructus Cnidii,Scorpio). METHODS: Fructus Cnidium and Scorpio were identified by TLC and the contents of icariine and osthole were determined by HPLC. RESULTS: Fructus Cnidium and Scorpio were clearly separated in the TLC chromatogram. The results of HPLC analysis for icariine were: a linear range of 61. 7 ng-740. 4 ng,r = 0. 999 6,an average recovery of 9... |
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| Keywords: | Ruxinan Capsule icariine osthole TLC HPLC |
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