| 乳康酊的薄层鉴别及丹皮酚的含量测定 |
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| 引用本文： | 刘智生,李嘉,黄建猷,黄瑞松.乳康酊的薄层鉴别及丹皮酚的含量测定[J].中国实验方剂学杂志,2011,17(2):50-52. |
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| 作者姓名： | 刘智生 李嘉 黄建猷 黄瑞松 |
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| 作者单位： | 1. 广西中医药研究院,南宁,530022
2. 广西民族医药研究所,南宁,530001 |
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| 基金项目： | 广西科技厅科技攻关项目(桂科攻0325002) |
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| 摘 要： | 目的:建立乳康酊薄层鉴别和含量测定的方法。方法:采用薄层色谱法对乳康酊中徐长卿、龙血竭进行定性鉴别;采用高效液相色谱法测定制剂中丹皮酚的含量。结果:在薄层色谱中可检出徐长卿和龙血竭;丹皮酚在0.03～0.27 g.L-1与峰面积呈良好的线性关系(r=0.999 9),平均加样回收率为99.01%,RSD 2.22%(n=6)。结论:所建立的方法简便、准确、可靠,可用于该制剂的质量控制。
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| 关 键 词： | 乳康酊 薄层色谱法 徐长卿 龙血竭 高效液相色谱法 丹皮酚 |
| 收稿时间： | 9/3/2010 12:00:00 AM |
Identification and Determination of Paeonol of Rukang Tincture |
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| LIU Zhi-sheng,LI Ji,HUANG Jian-you and HUANG Rui-song.Identification and Determination of Paeonol of Rukang Tincture[J].China Journal of Experimental Traditional Medical Formulae,2011,17(2):50-52. |
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| Authors: | LIU Zhi-sheng LI Ji HUANG Jian-you and HUANG Rui-song |
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| Institution: | LIU Zhi-sheng1,LI Jia1,HUANG Jian-you1,HUANG Rui-song2(1.Guangxi Institute of Traditional Medical and Pharmaceutical Sciences,Nanning 530022,China,2.Guangxi Institute of Minotity Nationalitu Medicine and Pharacology,Nanning 530001,China) |
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| Abstract: | Objective: To establish an identification and conten determination methods of Rukang Tincture. Method: Radix Cynanchi Paniculati and Resina Draconis were identified by TLC.The content of paeonol in Rukang tincture was determined by HPLC. Result: Radix Cynanchi Paniculati and Resina Draconis could be detected by TLC.Determine the content of paeonol by HPLC,paeonol showed a good linear relationship at a range of 0.03-0.27 g ·L-1 (r=0.999 9).The average recovery rate was 99.01% with RSD of 2.22% (n=6). Conclusion: The established methods are simple,accurate,reliable and can be used for the quality control of Rukang tincture. |
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| Keywords: | Rukang tincture TLC Radix Cynanchi Paniculati Resina Draconis HPLC paeonol |
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