| 青蛇藤化学成分研究 |
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| 引用本文： | 谭小鸿,张援虎,周岚,张洪金,谭明春,孙黔云,郝小江. 青蛇藤化学成分研究[J]. 中国药房, 2010, 0(47): 4463-4465 |
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| 作者姓名： | 谭小鸿 张援虎 周岚 张洪金 谭明春 孙黔云 郝小江 |
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| 作者单位： | [1]贵州省中国科学院天然产物化学重点实验室,贵阳市550002 [2]重庆市江北区精神卫生中心,重庆市400025 |
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| 基金项目： | 973计划前期研究专项项目课题（2009CB526512）; 贵州省中药现代化科技产业研究开发专项项目（黔科合农字[2006]5041号）; 贵州省科学技术基金项目（黔科合丁字[2006]2090号） |
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| 摘 要： | 目的:研究青蛇藤的化学成分。方法:应用硅胶、Sephadex LH-20、MCI、RP-18柱色谱对青蛇藤进行分离、纯化,根据理化常数和光谱分析鉴定其结构。结果:从青蛇藤氯仿萃取部分分离鉴定了8个单体化合物,分别为:杠柳苷(1)、杠柳苷元(2)、periplocoside M(3)、2α,3β,23-三羟基-乌苏-12-烯-28-羧酸(4)、北五加皮苷E(5)、熊果酸(6)、β-谷甾醇(7)和胡萝卜苷(8)。结论:化合物2、3、4为首次从该植物中分离得到。
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| 关 键 词： | 青蛇藤 化学成分 光谱分析 |
Study on Chemical Constituents of Periploca calophylla |
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| TAN Xiao-hong,ZHANG Yuan-hu,ZHOU Lan,TAN Ming-chun,SUN Qian-yun,HAO Xiao-jiang. Study on Chemical Constituents of Periploca calophylla[J]. China Pharmacy, 2010, 0(47): 4463-4465 |
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| Authors: | TAN Xiao-hong ZHANG Yuan-hu ZHOU Lan TAN Ming-chun SUN Qian-yun HAO Xiao-jiang |
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| Affiliation: | (Guizhou Province Key Laboratory for Chemistry of Natural Products of Chinese Academy of Sciences, Guiyang 550002, China) TAN Xiao-hong,ZHANG Hong-jin(Chongqing Jiangbei District Center for Mental Health,Chongqing 400025,China) |
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| Abstract: | OBJECTIVE： To study the chemical constituents of Periploca calophylla. METHODS： The samples were separated and purified on silica gel, Sephadex LH-20, MCI, RP-18 column. Their structures were identified by spectral and chemical methods. RESULTS： Eight compounds were isolated from the chloroform part of P. calophylla, including periplocin （1）, periplogenin （2）, periplocoside M （3）, 2α, 3β,23 trihydroxy ursolu 12 ene 28 carboxylic acid （4）, glycoside E （5）, ursolic acid （6）,β-sitosterol （7）, daucosterol（8）. CONCLUSION： Compounds 2,3 and 4 are isolated from P. calophylla for the first time. |
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| Keywords: | Periploca calophylla Chemical constituents Spectrum analysis |
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