| HPLC法测定壮骨关节丸中淫羊藿苷含量 |
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| 引用本文： | 阎小青. HPLC法测定壮骨关节丸中淫羊藿苷含量[J]. 天津医科大学学报, 2006, 12(2): 276-277,286 |
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| 作者姓名： | 阎小青 |
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| 作者单位： | 天津市天津医院药剂科,天津,300211 |
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| 摘 要： | 目的:建立高效液相色谱法(HPLC)测定壮骨关节丸中淫羊藿苷含量的方法。方法:采用HPLC法测定壮骨关节丸中淫羊藿苷的含量,以C18柱作为色谱柱,甲醇-1%冰醋酸(60:40)为流动相,检测波长为270 nm,按外标表法定量。结果:壮骨关节丸中淫羊藿苷的含量为0.498 7 mg/g。加样平均回收率为100.02%,RSD=1.58%(n=5);重现性试验的RSD=1.65%(n=6)。结论:为壮骨关节丸中药物的定性与定量分析提供了准确、灵敏的方法。
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| 关 键 词： | 壮骨关节丸 淫羊藿苷 高效液相色谱法 |
| 文章编号： | 1006-8147（2006）02-0276-03 |
| 收稿时间： | 2006-04-17 |
| 修稿时间： | 2006-04-17 |
HPLC method of controlling quality for Icariin in Zhuanggu Guanjie Pill |
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| YAN Xiao-qing. HPLC method of controlling quality for Icariin in Zhuanggu Guanjie Pill[J]. Journal of Tianjin Medical University, 2006, 12(2): 276-277,286 |
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| Authors: | YAN Xiao-qing |
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| Affiliation: | Pharmaceutical preparation section,Tianjin Hospital ,Tianjin 300211, China |
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| Abstract: | Objective: To study the method of controlling quality for Zhuanggu Guanjie Pill.Methods: Icariin in Zhuanggu Guanjie Pill was determined by HPLC,mobile phase was methanol-1% glacial acetic acid(60:40),detective wave length was 270 nm.Results: The icariin in Zhuanggu Guanjie Pill was 0.4987mg/g.The mean recovery was 100.02%,RSD=1.58%(n=5).RSD as repeatability index was 1.65%(n=6).Conclusion: The methods are available with a good reproducibility and can be used to control the quality of Zhuanggu Guanjie Pill. |
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| Keywords: | Zhuanggu Guanjie Pill Icariin HPLC |
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