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| 土木香根中土木香内酯和异土木香内酯的微波辅助提取工艺优化 | |
| 引用本文： | 赵永明,张敬,王哲,王宏霞,商兰兰,郭春燕,张万明.土木香根中土木香内酯和异土木香内酯的微波辅助提取工艺优化[J].中国实验方剂学杂志,2013,19(8):30-33. |
| 作者姓名： | 赵永明 张敬 王哲 王宏霞 商兰兰 郭春燕 张万明 |
| 作者单位： | 1. 河北北方学院药学系,河北张家口,075000 2. 河北北方学院附属第一医院肿瘤内科,河北张家口,075000 3. 河北北方学院附属第一医院泌尿科,河北张家口,075000 |
| 基金项目： | 河北省中医药管理局资助项目(2010046) |
| 摘 要： | 目的:优选微波法提取土木香根中土木香内酯和异土木香内酯的工艺条件.方法:以土木香内酯和异土木香内酯含量为指标,通过单因素试验和正交试验考察乙醇体积分数、料液比、微波辐射时间和提取温度等因素对提取工艺的影响,采用HPLC测定指标成分含量.结果:土木香内酯和异土木香内酯的最佳微波提取工艺为乙醇体积分数90％,料液比1∶15,微波时间180s,提取温度45℃.结论:优选的微波提取工艺具有稳定可行、节约时间、能耗低等优点. |
| 关 键 词： | 土木香 微波提取 正交设计 土木香内酯 异土木香内酯 |
| 收稿时间： | 2012/9/25 0:00:00 |
Optimization of Microwave-assisted Extraction Technology for Alantolactone and Isoalantolactone from Inula helenium Roots |
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| ZHAO Yong-ming,ZHANG Jing,WANG Zhe,WANG Hong-xi,SHANG Lan-lan,GUO Chun-yan and ZHANG Wan-ming.Optimization of Microwave-assisted Extraction Technology for Alantolactone and Isoalantolactone from Inula helenium Roots[J].China Journal of Experimental Traditional Medical Formulae,2013,19(8):30-33. | |
| Authors: | ZHAO Yong-ming ZHANG Jing WANG Zhe WANG Hong-xi SHANG Lan-lan GUO Chun-yan and ZHANG Wan-ming |
| Institution: | Department of Pharmacy, Hebei North University, Zhangjiakou 075000, China;Department of Oncology, The First Attached Hospital of Hebei Northern Institute, Zhangjiakou 075000, China;Department of Urology, The First Attached Hospital of Hebei Northern Institute, Zhangjiakou 075000, China;Department of Pharmacy, Hebei North University, Zhangjiakou 075000, China;Department of Pharmacy, Hebei North University, Zhangjiakou 075000, China;Department of Pharmacy, Hebei North University, Zhangjiakou 075000, China;Department of Pharmacy, Hebei North University, Zhangjiakou 075000, China |
| Abstract: | |
| Keywords: | Inula helenium microwave-assisted extraction orthogonal design alantolactone isoalantolactone |
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