| HPLC同时测定苦豆子总碱中8种生物碱含量 |
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| 引用本文： | 刘振龙,张丽,魏蕾初,郑堰心,邓虹珠. HPLC同时测定苦豆子总碱中8种生物碱含量[J]. 中国实验方剂学杂志, 2013, 19(8): 142-145 |
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| 作者姓名： | 刘振龙 张丽 魏蕾初 郑堰心 邓虹珠 |
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| 作者单位： | 1. 广东省食品药品检验所,广州 510180;南方医科大学中医药学院,广州 510515
2. 南方医科大学中医药学院,广州,510515 |
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| 摘 要： | 目的:建立苦豆子总碱中生物碱的含量测定方法.方法:采用HPLC,乙腈-0.05 mol· L-1磷酸二氢钾(三乙胺调pH ＞6.45),梯度洗脱,柱温35℃,检测波长205 nm,流速1.0 mL·min-1.结果:8种生物碱分离良好,8种生物碱含量＞50％.结论:该方法简便,可以作为苦豆子总碱的含量测定方法,比原标准中的滴定法测定总碱含量更方便、精确.
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| 关 键 词： | 苦豆子总碱 野靛碱 苦豆碱 槐定碱 氧化苦参碱 氧化槐果碱 槐果碱 苦参碱莱曼碱 含量测定 |
| 收稿时间： | 2012-07-10 |
HPLC Method for Simultaneous Determination of 8 Kinds of Alkaloids in Total Alkaloids of Sophora Alopecuroides |
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| LIU Zhen-long,ZHANG Li,WEI Lei-chu,ZHENG Yan-xin and DENG Hong-zhu. HPLC Method for Simultaneous Determination of 8 Kinds of Alkaloids in Total Alkaloids of Sophora Alopecuroides[J]. China Journal of Experimental Traditional Medical Formulae, 2013, 19(8): 142-145 |
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| Authors: | LIU Zhen-long ZHANG Li WEI Lei-chu ZHENG Yan-xin DENG Hong-zhu |
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| Affiliation: | Guangdong Insititute for Food and Drug Control, Guangzhou 510180, China;College of Traditional Chinese Medicine, Southern Medical University, Guangzhou 510515, China;College of Traditional Chinese Medicine, Southern Medical University, Guangzhou 510515, China;College of Traditional Chinese Medicine, Southern Medical University, Guangzhou 510515, China;College of Traditional Chinese Medicine, Southern Medical University, Guangzhou 510515, China;College of Traditional Chinese Medicine, Southern Medical University, Guangzhou 510515, China |
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| Abstract: | |
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| Keywords: | total alkaloids in sophora alopecuroides cytisine aloperine sophoridine oxymatrine oxysophocarpine sophocarpine matrine lehmannine content determination |
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