| 悬浮液进样技术-原子荧光光谱法测定中成药中痕量砷、锑、硒和镉的分析方法及其干扰效应的研究 |
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| 引用本文： | 林建原,黄志勤. 悬浮液进样技术-原子荧光光谱法测定中成药中痕量砷、锑、硒和镉的分析方法及其干扰效应的研究[J]. 赣南医学院学报, 2002, 22(4): 337-339 |
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| 作者姓名： | 林建原 黄志勤 |
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| 作者单位： | 赣南医学院化学教研室,江西,赣州,341000 |
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| 摘 要： | 目的：利用悬浮液进样技术-原子荧光光谱法测定中成药中痕量砷，锑，硒和镉的分析方法。方法：将样品粉碎，过筛制备成琼脂，加入硫脲-抗坏血酸消除共存离子的干扰。结果：该方法快速，灵敏干扰少，标准回收率在93.3%-100.0%之间。结论：该方法用于测定中成药中痕量砷，锑，硒和镉，结果令人满意。
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| 关 键 词： | 砷 锑 硒 镉 干扰效应 悬浮液进样 原子荧光光谱法 中成药 痕量元素 中药质量 |
| 文章编号： | 1001-5779(2002)04-0337-03 |
| 修稿时间： | 2002-03-04 |
A Study of the Suspension Sampling-Atomic Fluorescence Spectrometric Tetermination of Trace As, Sb,Se and Cd in Chinese Traditional Medicines |
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| LIN Jian yuan,et al. A Study of the Suspension Sampling-Atomic Fluorescence Spectrometric Tetermination of Trace As, Sb,Se and Cd in Chinese Traditional Medicines[J]. Journal of Gannan Medical College, 2002, 22(4): 337-339 |
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| Authors: | LIN Jian yuan et al |
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| Abstract: | Objective :A method for The Suspension Sampling -Atomic Fluorescence Spectrometric Tetermination Of Trace As,Sb,Se and Cd in Chinese Traditional Medicines.Method: The samples were pulverized and suspended in agar sol.Test solutions were preparered by adding thiourea and vitamin C to eliminate chemical interference.Results:The Proposed method is fast, convenient and has less interferences.The recovery is 93.3%-100.0%.Conclusion:The method has been used to determine trace As,Sb,Se and Cd in Chinese Traditional Medicines with satisfactory results. |
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| Keywords: | Suspension Sampling Chinese Traditional Medicines Atomic Fluorescence Spectrometric |
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