| 乳康胶囊质量标准研究 |
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| 引用本文： | 叶延程,赵良存.乳康胶囊质量标准研究[J].中国实验方剂学杂志,2012,18(13):125-128. |
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| 作者姓名： | 叶延程 赵良存 |
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| 作者单位： | 甘肃省武威肿瘤医院,甘肃武威,733000 |
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| 摘 要： | 目的:建立乳康胶囊的质量控制方法.方法:对乳康胶囊中青皮、柴胡进行薄层色谱鉴别；采用HPLC对柴胡皂苷a、柴胡皂苷d进行总含量测定.结果:薄层色谱斑点清晰,阴性对照无干扰；柴胡皂苷a进样量在2.04～ 14.28 μg(r=0.999 8)、柴胡皂苷d进样量在2.52-17.64 μg(r =0.9995)线性关系良好.平均回收率为99.15％,RSD 0.54％ (n =9).结论:建立的TLC和HPLC专属性强、准确度高、重复性好,可用于乳康胶囊的质量控制.
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| 关 键 词： | 乳康胶囊 质量标准 高效液相色谱法 柴胡皂苷a 柴胡皂苷d |
| 收稿时间： | 2011/12/22 0:00:00 |
Quality Standard of Rukang Capsule |
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| YE Yan-cheng and ZHAO Liang-cun.Quality Standard of Rukang Capsule[J].China Journal of Experimental Traditional Medical Formulae,2012,18(13):125-128. |
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| Authors: | YE Yan-cheng and ZHAO Liang-cun |
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| Institution: | Department of Pharmacy, Gansu Wuwei Tumor Hospital, Wuwei 733000, China;Department of Pharmacy, Gansu Wuwei Tumor Hospital, Wuwei 733000, China |
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| Abstract: | Objective:To established the method for quality control of Rukang capsule.Method: Citri Reticulatae Pericarpium viride,Bupleuri Radix in Rukang capsule were identified by TLC.The content of saikosaponin a and Saikosaponin d in Rukang Capsule was determined by HPLC.Result: The spots on the TLC plate were clear and the negative control sample didn’t disturb.A good linearity was obtained for saikosaponin a in the range of 2.04-14.28 μg(r=0.999 8)and saikosaponin d in the range of 2.52-17.64 μg(r=0.999 5).The average recovery was 99.15%(RSD 0.54%,n=9).Conclusion:The method are specific,accurate and reproducible,and can be used for quality control of Rukang capsule. |
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| Keywords: | Rukang capsule quality standard HPLC saikosaponin a saikosaponin d |
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