| 山东肿足蕨高效液相色谱指纹图谱初步研究 |
| |
| 引用本文： | 张华丽,朱军,高桂花. 山东肿足蕨高效液相色谱指纹图谱初步研究[J]. 济宁医学院学报, 2011, 0(6): 389-391 |
| |
| 作者姓名： | 张华丽 朱军 高桂花 |
| |
| 作者单位： | 济宁医学院药学院; |
| |
| 基金项目： | 济宁医学院2008年青年科研基金项目 |
| |
| 摘 要： | 目的 建立山东肿足蕨药材的高效液相色谱指纹图谱,为其质量控制提供参考.方法 采用高效液相色谱(HPLC)法,色谱柱VP-ODS,流速1 ml/min,检测波长215nm,柱温25℃,用乙腈和水作为流动相,梯度洗脱,测定了10批山东肿足蕨样品.结果 得到了山东肿足蕨HPLC指纹图谱.结论 用文中的最佳条件可较全面地反映山...
|
| 关 键 词： | 山东肿足蕨 高效液相色谱法 指纹图谱 |
HPLC Fingerprint Spectrum of Hypodematium sinense lwatsuki |
| |
| ZHANG Hua-li,ZHU Jun,GAO Gui-hua. HPLC Fingerprint Spectrum of Hypodematium sinense lwatsuki[J]. Jounal of Jinning Medical College, 2011, 0(6): 389-391 |
| |
| Authors: | ZHANG Hua-li ZHU Jun GAO Gui-hua |
| |
| Affiliation: | ZHANG Hua-li,ZHU Jun,GAO Gui-hua(Pharmaceutical college,Jining Medical University,Rizhao 276826,China) |
| |
| Abstract: | Objective HPLC fingerprint spectrum of Hypodematium Sinense Iwatsuri was established in order to provide reference for its quality control.Methods RP-HPLC （DAD） was used in the determination of Hypode- matium Sinense Iwatsuri by gradient elution under the following condition： column of VP-ODS, flow rate of lmL/ rain,detection wavelength of 215 nm, temperature of 25℃ and acetonitrile and water as mobile phase, 10 batches of Hypodematium Sinense Iwatsuri were determined.Results A preferable method for HPLC fingerprint determina- tion of the Hypodematium Sinense Iwatsuri was established. Conclusion A general acquaintance of the Hypodematium Sinense Iwatsuri can be obtained by using the preferable HPLC fingerprint determination method, which is useful for quality valuation of the Hypodematium Sinense Iwatsuri. |
| |
| Keywords: | Hypodematium Sinense Iwatsuri HPLC Fingerprint Spectrum |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
