| 抗风湿类中成药中非法添加布洛芬的快速测定 |
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| 引用本文： | 李蔚,陈日檬,沈彩云. 抗风湿类中成药中非法添加布洛芬的快速测定[J]. 药学研究, 2017, 36(3): 138-141,169. DOI: 10.13506/j.cnki.jpr.2017.03.004 |
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| 作者姓名： | 李蔚 陈日檬 沈彩云 |
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| 作者单位： | 湛江市食品药品检验所,广东 湛江,524022 |
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| 基金项目： | 广东药检系统科研项目(YJ201228) |
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| 摘 要： | 目的 建立快速筛查抗风湿类中成药中非法添加布洛芬的薄层色谱方法.方法 样品经甲醇提取,采用硅胶GF254薄层板,水饱和的乙酸乙酯为展开剂,在紫外光灯(254 nm)下检测.结果 该实验方法简单,经济,快速,薄层色谱分离效果好.结论 薄层色谱法可对抗风湿类中成药中非法添加布洛芬进行快速的测定,加强对该类产品的监督检查.
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| 关 键 词： | 布洛芬 薄层色谱 非法添加 快速测定 |
Rapid determination of illegally added ibuprofen in anti-rheumatic traditional Chinese medicine |
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| LI Wei,CHEN Rimeng and SHEN Caiyun. Rapid determination of illegally added ibuprofen in anti-rheumatic traditional Chinese medicine[J]. Journal of Pharmaceutical Research, 2017, 36(3): 138-141,169. DOI: 10.13506/j.cnki.jpr.2017.03.004 |
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| Authors: | LI Wei CHEN Rimeng SHEN Caiyun |
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| Affiliation: | Zhanjiang Institute for Food and Drug Control,Zhanjiang 524022,China,Zhanjiang Institute for Food and Drug Control,Zhanjiang 524022,China and Zhanjiang Institute for Food and Drug Control,Zhanjiang 524022,China |
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| Abstract: | Objective To establish a TLC method for rapid determination of ibuprofen that added to anti-rheumatic traditional Chinese medicine illegally.Methods Samples were methanol extracted,using silica gel GF254 thin layer plate,water-saturated ethyl acetate as expansion agent,detecting at 254 nm.Results This method was simple,economic,rapid and the separation result of TLC was really nice.Conclusion TLC can be used to determine the ibuprofen rapidly that added to the anti-rheumatic traditional Chinese medicine.In order to strengthen the supervision and inspection of the product. |
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| Keywords: | Ibuprofen TLC Illegally added Rapid determination |
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