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| 复方雪莲滴丸中羌活、独活的纯化工艺考察 | |
| 引用本文： | 罗玉琴 杨伟俊 徐建国 邢建国. 复方雪莲滴丸中羌活、独活的纯化工艺考察[J]. 中国中药杂志, 2008, 33(21): 2478-2478 |
| 作者姓名： | 罗玉琴 杨伟俊 徐建国 邢建国 |
| 作者单位： | 1. 中国科学院新疆理化技术研究所,新疆,乌鲁木齐,830011 2. 新疆维吾尔自治区药物研究所,新疆,乌鲁木齐,830004 |
| 摘 要： | 目的：考察复方雪莲滴丸中羌活、独活提取物的大孔树脂纯化工艺。方法：以蛇床子素和异欧前胡素为指标，对树脂型号、上样量、洗脱溶剂进行了筛选；考察了上样液浓度、上样液pH、柱径高比对吸附的影响。结果：选择HPD400A大孔树脂，树脂体积与上样量体积比1∶2，pH 3.5(原液)，柱径高比1∶7，洗脱溶剂95%乙醇时，解吸效果较好。结论：可以应用HPD400A大孔树脂纯化羌活、独活提取物。 |
| 关 键 词： | 复方雪莲滴丸 羌活 独活 大孔吸附树脂 纯化 |
| 收稿时间： | 1900-01-01 |
| 修稿时间： | 1900-01-01 |
Purification technology of Rhizoma et Radix Notopterygii and Radix Angelicae Pubescentis in Fufang Xuelian dropping pills by macroporous resin |
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| LUO Yu-qin; YANG Wei-jun; XU Jian-guo; XING Jian-guo. Purification technology of Rhizoma et Radix Notopterygii and Radix Angelicae Pubescentis in Fufang Xuelian dropping pills by macroporous resin[J]. China Journal of Chinese Materia Medica, 2008, 33(21): 2478-2478 |
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| Authors: | LUO Yu-qin YANG Wei-jun XU Jian-guo XING Jian-guo |
| Abstract: | Objective:To study the purification technology of Rhizoma et Radix Notopterygii and Radix Angelicae Pubescentis in Fufang Xuelian dropping pills by macroporous resin.Method:Taking osthole,isomperatorin as index ingredients,the type of resin sampling amount and elution solvent were decided,and the influence of sample concentration pH of sample and ratio of diameter to height of collumn to adsorption were studied.Result:HPD400A was chosen to purify,the suitable sampling ratio of resin volum to raw material wa... |
| Keywords: | Fufang Xuelian dropping pills Rhizoma et Radix Notopterygii Radix Angelicae Pubescentis macroporous absorption resin purification |
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