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萃取法分离提纯乙二醛中的乙醛酸
引用本文:胡军 张新胜 等. 萃取法分离提纯乙二醛中的乙醛酸[J]. 医学教育探索, 2001, 0(4): 334-337
作者姓名:胡军 张新胜 等
作者单位:[1]华东理工大学联合化学反应工程研究所反应工程国家重点实验室,上海200237 [2]华东理工大学联合化学反应工程研究
基金项目:全军医药卫生科研基金课题(编号98M143)
摘    要:乙二醛阳极电氧化制乙醛酸工艺中,乙醛酸的纯化问题直接关系到电流效率及产品质量,采用萃取法除去乙醛酸中的乙二醛。分别研究了叔胺类萃取剂,稀释剂、萃洗剂的组成和配方、以及最佳萃取工艺条件,使电解液中乙醛酸与乙二醛的质量比由(3-2:1)纯化为(30-20:1)。

关 键 词:乙醛酸 乙二醛 叔胺 萃取工艺 反萃取 萃取剂 稀释剂 萃洗剂 电流效率

Extraction of Glyoxalic Acid from Aqueous Mixture with Glyoxal
HU Jun,ZHANG Xin sheng,ZHOU Yang liu,DAI Ying chun. Extraction of Glyoxalic Acid from Aqueous Mixture with Glyoxal[J]. Researches in Medical Education, 2001, 0(4): 334-337
Authors:HU Jun  ZHANG Xin sheng  ZHOU Yang liu  DAI Ying chun
Abstract:Object To explore the bacteriostatic and anti inflammation activities of ultrasonically nebulized Houttuynai cordata Thunb in patients after pneumonectomy Methods The patients were randomized into 2 groups Patients of the experimental group, inhaled ultrasonically nebulized H cordata, while patients in the control group inhaled ultrasonically nebulized vapors without the addition of H cordata Results Total leucocyte counts on the third and fourth day in the experimental group were significantly lower than that in the control group Neutrophil ratio in experimental group was also lower in all the 5 days of treatment although nonsignificantly Meanwhile, occurrence of Gram negative bacilli colonization in experimental group occurred less than that in the control group But incidence of fungi colonization appeared higher Conclusion Inhalation of ultrasonically nebulized H cordata can ease the inflammation and inhibit the colonization of Gram negative bacilli in respiratory tract
Keywords:glyoxalic acid  glyoxal  tertiary amine  extraction  stripping
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