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不同产地马尾松针挥发油的GC—MS分析
引用本文:李洪玉,寿旦,李亚平,俞忠明,章建民.不同产地马尾松针挥发油的GC—MS分析[J].中医药学刊,2011(1):78-81.
作者姓名:李洪玉  寿旦  李亚平  俞忠明  章建民
作者单位:浙江省中医药研究院,浙江杭州310007
基金项目:基金项目:浙江省科技计划资助项目(2008F10G5260007)
摘    要:目的:对不同产地的马尾松针挥发油成分进行分析比较,探讨不同产地样品的成分组成及含量差异。方法:采集全国5个省份的马尾松针,采用水蒸气蒸馏法提取挥发油,利用气相色谱一质谱(GC/MS)联用技术,分别对5种松针挥发油的化学成分进行分析。结果:从五地的马尾松松针挥发油中分离鉴定出多种化学成分,其中石竹烯,(Z,Z,Z)-1,5,9,9四-甲基-1,4,7环-十一碳三烯,(+)-表双环倍半水芹烯等7种总含量超过挥发油20%的成分为共有组分。结论:不同产地马尾松针挥发油的主要化学成分较为相似,主要是单萜和倍半萜,但在含量上有较大的差别。

关 键 词:GC—MS  马尾松针挥发油

Comparison Analysis of Volatile Constituents of Pine Needles from Pinus Massoniana Lamb Planted in Different Area by GC- MS
LI Hong-yu,SHOU Dan,YU Zhong-ming,ZHANG Jian-min.Comparison Analysis of Volatile Constituents of Pine Needles from Pinus Massoniana Lamb Planted in Different Area by GC- MS[J].Study Journal of Traditional Chinese Medicine,2011(1):78-81.
Authors:LI Hong-yu  SHOU Dan  YU Zhong-ming  ZHANG Jian-min
Institution:(Zhejiang Academy of Traditional Chinese medicine, Hangzhou 310007, Zhejiang,China)
Abstract:Objective: The volatile constituents of pine needles from pinus massoniana lamb planted in different area were analyzed to research the constituents difference among the samples from different area.Methods: Pine needles from pinus massoniana lamb were gathered from 5 province,and the oil were extracted through steam distillation.Volatile oil were analyzed by gas—chromatography—mass spectrometry.Results: There were various compositions identified from every oil sample,and 7 oil compositions including Caryophyllene、(Z,Z,Z)-1,5,9,9-tetramethyl-1,4,7-cycloundecatriene、(+)-Epi-bicyclosesquiphellandrene and so on were contained in total 5 samples.Conclusion:The results reveal that the essential oil compositions of pine needles from pinus massoniana lamb planted in different area were similar but the contents of some compounds different greatly.
Keywords:GC - MS  volatile constituents of pine needles from pinus massoniana Lamb
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