| 黄芩中汉黄芩素的提取制备 |
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| 引用本文： | 李文娟,潘馨,陈晓兰,陈维中,廖联明.黄芩中汉黄芩素的提取制备[J].亚太传统医药,2014(9):33-35. |
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| 作者姓名： | 李文娟 潘馨 陈晓兰 陈维中 廖联明 |
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| 作者单位： | [1]福建中医药大学,福建福州350122 [2]南京军区福州总医院第一附属医院,福建莆田351100 |
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| 摘 要： | 为建立制备大量高纯度汉黄芩素的方法,将中药黄芩50g用pH 5水水解12h,再用95％的乙醇提取,得到的提取物浸膏,过30～60目的聚酰胺树脂柱纯化,将含有汉黄芩素的洗脱物采用高速逆流色谱（HSCCC）进行分离.通过该方法制得汉黄芩素525mg,纯度为98.7％.
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| 关 键 词： | 汉黄芩素 黄芩 提取 聚酰胺柱 纯化 高速逆流色谱 |
Extraction and Preparation of Wogonin from Radix Scutellariae |
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| Li Wenjuan,Pan Xin,Chen Xiaolan,Chen Weizhong,Liao Lianming.Extraction and Preparation of Wogonin from Radix Scutellariae[J].Asia-Pacific Traditional Medicine,2014(9):33-35. |
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| Authors: | Li Wenjuan Pan Xin Chen Xiaolan Chen Weizhong Liao Lianming |
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| Institution: | 1. Fujian University of Traditional Chinese Medicine, Fuzhou 350122, China; 2. Fuzhou General Hospital of Nanjing Military Region, the First Affiliated Hospital, Fujian 350122,China) |
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| Abstract: | To develop a method for large scale preparation of high-purity Wogonin from Radix Scutellariae. 50g of Radix Scutellariae was hydrolyzed in water （pH 5） for 12h, and then extracted with 95% ethanol. The extractum was seperated with 30 - 60 mesh polyamide resin column. Fraction with Wogonin was subjected to high-speed countercurrent chromatography （HSCCC） . 525mg Wogonin is obtained with a purity 98.7 %. Thus an effective method for preparing high-purity Wogonin was established. |
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| Keywords: | Wogonin Radix Scutellariac Extraction Polyamide Resin Column Purifion HSCCC |
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