| 大孔吸附树脂法分离纯化化橘红中柚皮苷的研究 |
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| 引用本文： | 韦敏,杨中林,吴建民.大孔吸附树脂法分离纯化化橘红中柚皮苷的研究[J].中成药,2007,29(3):352-354. |
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| 作者姓名： | 韦敏 杨中林 吴建民 |
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| 作者单位： | 中国药科大学,江苏,南京,210038 |
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| 摘 要： | 目的:优选分离纯化柚皮苷的大孔吸附树脂。方法:以柚皮苷的吸附量和解吸率为考察指标,从中筛选研究大孔吸附树脂分离纯化柚皮苷的吸附性能和洗脱参数。结果:HPD450树脂对柚皮苷有较好的吸附分离效果,适合于化橘红中柚皮苷的提纯,经该树脂吸附解吸,饱和吸附量可达71.7mg/g,解吸率达95.8。结论:通过大孔树脂分离纯化后,终产品中柚皮苷的纯度可达85,证明采用本法分离纯化化橘红中柚皮苷是可行。
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| 关 键 词： | 化橘红 柚皮苷 大孔吸附树脂 分离纯化 |
| 文章编号： | 1001-1528（2007）03-0352-03 |
| 修稿时间： | 2006-02-15 |
Separation and purification of naringin from Citrus grandis Tomentosa by macroporous adsorption resin |
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| WEI Min,YANG Zhong-lin,WU Jian-min.Separation and purification of naringin from Citrus grandis Tomentosa by macroporous adsorption resin[J].Chinese Traditional Patent Medicine,2007,29(3):352-354. |
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| Authors: | WEI Min YANG Zhong-lin WU Jian-min |
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| Institution: | China Pharmaceutical University, Nanjing 210038, China |
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| Abstract: | AIM: To optimize the macroporous resin for separating naringin. METHODS: Putting the extract fluid of Citrus grandis Tomentosa into pillar was adsorbed with macroporous resin, then washed by alcohol with the different concentration in succession to determine the content of naringin by HPLC. RESULTS: The six macroporous resins' effects differ greatly. CONCLUSION: HPD450 macroporous resin is effective to separate the naringin. |
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| Keywords: | Citrus grandis Tomentosa naringin macroporous resin separation and purification |
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