| HPLC法测定豨莶风湿片中粉防己碱及防己诺林碱的含量 |
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| 引用本文： | 刘珊珊,殷善霞,张峰. HPLC法测定豨莶风湿片中粉防己碱及防己诺林碱的含量[J]. 现代中药研究与实践, 2011, 0(2): 74-76 |
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| 作者姓名： | 刘珊珊 殷善霞 张峰 |
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| 作者单位： | 山东大学附属省立医院;山东中医药大学; |
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| 摘 要： | 目的 建立豨莶风湿片中粉防己碱及防己诺林碱的HPLC测定方法.方法 色谱柱为C<,18>柱(4.6mm×l50 mm,5 μm);流动相为乙腈-水-三乙胺(70:30:0.01),流速为1.0 mL/min,检测波长为280nm.结果 粉防己碱及防已诺林碱的进样量分别在0.344 μg～1.72 μg(r=0.999 ...
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| 关 键 词： | HPLC法 豨莶风湿片 粉防己碱 防己诺林碱 |
Determination of Tetrandrine and Fangchinoline in Xixianfengshi Tablet by HPLC |
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| LIU Shan-shan,YIN Shan-xia,ZHANG Feng. Determination of Tetrandrine and Fangchinoline in Xixianfengshi Tablet by HPLC[J]. Research and Practice on Chinese Medicines, 2011, 0(2): 74-76 |
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| Authors: | LIU Shan-shan YIN Shan-xia ZHANG Feng |
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| Affiliation: | LIU Shan-shan1,YIN Shan-xia2,ZHANG Feng2(1.The Provincial Affiliated Hospital to Shandong University,Jinan 250021,China,2.Shandong University of Traditional Chinese Medicine,Jinan 250355,China) |
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| Abstract: | Objective To establish an HPLC method for the determination of tetrandrine and fangchinoline in Xixianfengshi tablets.Methods The method was performed on C18（4.6 mm×150 mm,5 μm） column with acetonitrile-water-triethylamin（70 ： 30 ： 0.1） as mobile phase.Flow rate was 1.0 mL/min,and the wavelength was 280 nm.Results The linear ranges of tetrandrine and fangchinoline were 0.344 μg~1.72 μg（r=0.999 9）,0.153 μg~0.765 μg（r=0.999 9）,respectively.The average recovery were 99.20% and 99.26%,respectively,Conclusion This method is proved to be simple,accurate and can be used for quality control of Xixianfengshi tablets. |
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| Keywords: | HPLC Xixianfengshi tablets fangchinoline tetrandrine |
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