| 三羟乙基芦丁对照品的制备 |
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| 引用本文： | 王厚全,任慧霞,王本杰,程秀民. 三羟乙基芦丁对照品的制备[J]. 中国药学杂志, 2004, 39(7): 548-549 |
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| 作者姓名： | 王厚全 任慧霞 王本杰 程秀民 |
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| 作者单位： | 山东大学药学院,山东,济南,250012 |
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| 摘 要： | 目的 制备三羟乙基芦丁对照品用于曲克芦丁的HPLC含量测定。方法 采用超越终点合成法减少产品中二羟乙基芦丁含量。结果 制备出符合要求的三羟乙基芦丁对照品并用于曲克芦丁质量标准的制订。结论 三羟乙基芦丁的纯度达到95.9%。
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| 关 键 词： | 芦丁 三羟乙基芦丁 对照品 制备 高效液相色谱法 |
| 文章编号： | 1001-2494(2004)07-0548-02 |
| 收稿时间： | 2003-03-17; |
Preparation of trihydroxyethylrutin refrence substance |
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| WANG Hou-quan,REN Hui-xia,WANG Ben-jie,Cheng Xiu-min. Preparation of trihydroxyethylrutin refrence substance[J]. Chinese Pharmaceutical Journal, 2004, 39(7): 548-549 |
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| Authors: | WANG Hou-quan REN Hui-xia WANG Ben-jie Cheng Xiu-min |
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| Affiliation: | College of Pharmacy, Shandong University, Jinan， 250012, China |
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| Abstract: | OBJECTIVE To prepare trihydroxyethylrutin refrence substance for the HPLC assay of troxerutin. METHODS The synthesis method of exceeding terminal point was adopted to reduce the content of dihydroxyethylrutin in the product. RESULTS Trihydroxyethylrutin refrence substance was prepared and used in working out the quality standard of troxerutin. CONCLUSION The purity of trihydroxyethylrutin is 95.9%. |
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| Keywords: | rutin trihydroxyethylrutin refrence substance preparation HPLC |
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