| 大孔吸附树脂分离纯化三七总皂苷工艺研究 |
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| 引用本文： | 石召华,熊富良,李崇明,王永平,陈鹏. 大孔吸附树脂分离纯化三七总皂苷工艺研究[J]. 中成药, 2004, 26(1): 10-12 |
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| 作者姓名： | 石召华 熊富良 李崇明 王永平 陈鹏 |
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| 作者单位： | 1. 湖北中医学院,湖北,武汉,430061
2. 湖北省中药现代化技术研究中心,湖北,武汉,430052 |
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| 基金项目： | 湖北省武汉市青年科技晨光计划 |
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| 摘 要： | 目的:研究大孔吸附树脂法纯化三七总皂苷的工艺条件及参数.方法:以三七总皂苷的量为考察指标,研究树脂吸附容量、洗脱溶媒及其用量,并用正交实验法优选最佳洗脱条件.结果:通过大孔吸附树脂纯化后,70%乙醇洗脱液干燥后总固物中三七总皂苷纯度可达83.3%.结论:采用此法能较好的纯化三七总皂苷.
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| 关 键 词： | 大孔吸附树脂 三七总皂苷 分离纯化 |
| 文章编号： | 1001-1528(2004)04-0010-03 |
Studies on separation and purification of total arasaponin with macroporous resin |
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| SHI Zhao-hua ,XIONG Fu-liang ,LI Chong-ming ,WANG Yong-ping ,CHEN Peng. Studies on separation and purification of total arasaponin with macroporous resin[J]. Chinese Traditional Patent Medicine, 2004, 26(1): 10-12 |
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| Authors: | SHI Zhao-hua XIONG Fu-liang LI Chong-ming WANG Yong-ping CHEN Peng |
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| Affiliation: | SHI Zhao-hua 1,XIONG Fu-liang 2,LI Chong-ming 2,WANG Yong-ping 2,CHEN Peng 2 |
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| Abstract: | AIM: To optimize the technical parameters of total arasaponin'S purification with macroporous resin. METHODS: Conditions for the elution were studies under the conditio n of the content of total arasaponin. RESULTS: The purity of total arasaponin was up to 83.3% after d riing the part of 70% ethanolic elution. CONCLUSION: The method was a good purification for total arasaponi n. |
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| Keywords: | macroporous resin total arasaponin separation and purification |
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