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牛尾独活挥发油成分的GC-MS分析
引用本文:张才煜,张本刚,杨秀伟.牛尾独活挥发油成分的GC-MS分析[J].中国现代中药,2005,7(12):9-12.
作者姓名:张才煜  张本刚  杨秀伟
作者单位:1. 中国协和医科大学,中国医学科学研究院药用植物研究所,北京,100094
2. 北京大学药学院,天然药物及仿生药物国家重点实验室,北京大学医药卫生分析中心,北京,100083
摘    要:目的:分析牛尾独活(Heracleum hemsleyanum Diels的根)挥发油的化学成分.方法:采用水蒸气蒸馏法提取牛尾独活根挥发油,用GC毛细管色谱柱进行分离和分析,归一化法测定其相对含量,GC-MS法鉴定化学成分.结果:鉴定了53个化学成分.结论:牛尾独活挥发油中主要成分为:(1S)-6,6-二甲基-2-亚甲基3.1.1]-双环庚烷(12.60%)、8-异丙基-1,5-二甲基-环十碳1,5-二烯(10.42%)、匙叶桉油烯醇(7.63%)、正辛醇(7.3 5%)、3-甲基壬烷(4.28%),与其他品种独活挥发油中的主要成分有较大差别.

关 键 词:牛尾独活  挥发油
收稿时间:2005/10/14 0:00:00
修稿时间:2005年10月14

GC-MS Analysis of Essential Oil from the Radix of Heracleum hemsleyanum Diels
Zhang Caiyu,Zhang Bengang and Yang Xiuwei.GC-MS Analysis of Essential Oil from the Radix of Heracleum hemsleyanum Diels[J].Modern Chinese Medicine,2005,7(12):9-12.
Authors:Zhang Caiyu  Zhang Bengang and Yang Xiuwei
Institution:Institute of Medicinal Plant Development, Chinese Academy of Medical Science and Peking Union Medical College, Beijing 100094, China;;Institute of Medicinal Plant Development, Chinese Academy of Medical Science and Peking Union Medical College, Beijing 100094, China;;State Key Laboratory of Natural & Biomimetic Drugs, School of Pharmaceuti-cal Sciences, and Medical and Healthy Analysis Center, Peking University, Beijing 100083, China
Abstract:Objective: To Analyz the components of the essential oils extracted from the radix of Heracleum hemsleyanum Diels. Method: The essential oils were extracted by water-steam distillation and separated by capillary columns gas chromatography. The components were determined with area normalization method, and were identi- fied by GC-MS. Result: Fifty-three constituents were identified. Conclusion: The main components are (1S)-6,6- dimethyl-2-methylenebicyclo 3.1.1heptane (12.60%), 8-isopropenyl-1,5-dimethyl-cyclodeca-1,5 -diene (10.42%), spathulenol (7.63%), octanal (7.35%), and 3-methylnonane (4.28%). The essential oil has a lot of differences from other varieties Duhuo.
Keywords:GC-MS
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