| 高效液相色谱法测定感冒止咳冲剂中葛根素的含量 |
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| 引用本文： | 于立佐,王延龙. 高效液相色谱法测定感冒止咳冲剂中葛根素的含量[J]. 齐鲁药事, 2004, 23(3): 28-29 |
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| 作者姓名： | 于立佐 王延龙 |
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| 作者单位： | 1. 济宁市药品检验所,济宁,272025
2. 泗水县人民医院药剂科,泗水,273200 |
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| 摘 要： | 目的 测定感冒止咳冲剂中葛根素的含量。方法 采用高效液相色谱法,色谱柱为ODS -C18柱,流动相为甲醇～1 4 %醋酸溶液(2 2∶78)。检测波长为 2 5 0nm。结果 平均加样回收率为 99 87%,RSD =1 0 5 %(n =5)。结论 方法简便,重现性好,其它成分无干扰。提供了感冒止咳冲剂的质量控制方法。
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| 关 键 词： | 感冒止咳冲剂 葛根素 高效液相色谱法 |
| 文章编号： | 1672-7738(2004)03-0028-02 |
Determination of Kakonein in Ganmao Zhike Powder by HPLC |
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| Yu Li-zuo,Wang Yan-long. Determination of Kakonein in Ganmao Zhike Powder by HPLC[J]. qilu pharmaceutical affairs, 2004, 23(3): 28-29 |
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| Authors: | Yu Li-zuo Wang Yan-long |
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| Affiliation: | Yu Li-zuo,Wang Yan-long1 |
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| Abstract: | Objective Determination of Kakonein in Ganmao Zhike Powder by HPLC. Methods Column was ODS-C 18,with methanol-acetic acid (22∶78) as mobile phase.Determination wave-length was 250nm.Results The recovery rate of the added sample was 99.87%,RSD=1.05%(n=5).Conclusion This method is easy and showed high good reproducibility without distraction.This method is available for the quality control of Ganmao Zhike Powder. |
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| Keywords: | Ganmao Zhike Powder Kakonein HPLC |
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