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陆英颗粒质量标准研究
引用本文:汪玢,张宁,何京,涂剑平. 陆英颗粒质量标准研究[J]. 中国现代中药, 2007, 9(8): 15-16
作者姓名:汪玢  张宁  何京  涂剑平
作者单位:1. 南昌大学理学院化学系,江西,南昌,330006;南昌大学药学系,江西,南昌,330026
2. 南昌大学理学院化学系,江西,南昌,330006
3. 南昌大学药学系,江西,南昌,330026
摘    要:目的:建立陆英颗粒的质量标准。方法:采用薄层色谱法鉴别熊果酸,并应用UV测定以芦丁计总黄酮的含量。结果:TLC法专属性强,含量测定以芦丁计总黄酮在0.008~0.065mg.mL^-1呈良好的线性关系,平均回收率为98.58%,RSD=0.34%。结论:本质量标准可有效地控制陆英颗粒的质量,且方法稳定、简便可行。

关 键 词:陆英颗粒  质量标准  黄酮  薄层色谱法  含量测定
收稿时间:2007-02-06
修稿时间:2007-02-06

Studies On Quality Standard of Sambucus chinensis Lindl. Granules
Wang Bin,Zhang Ning,He Jing and Tu Jian Ping. Studies On Quality Standard of Sambucus chinensis Lindl. Granules[J]. Modern Chinese Medicine, 2007, 9(8): 15-16
Authors:Wang Bin  Zhang Ning  He Jing  Tu Jian Ping
Affiliation:Chemistry department in Science College of Nanchang Universtry, Nanchang Jiangxi 330006, China ; 2. Pharmacy College of Nanchang Universtry , Nanchang Jiangxi 330026, China
Abstract:Objective:To establish the quality standard of Sambucus chinensis Lindl.granules. Methods:TLC was used for simultaneous identification of arsolic acid , UV was used for the determination of all flavonoids depending on rutin. Results: The TLC identification was highly specific and the spots was clear. The linearity for all flavonoids depending on rutin was obtained over the range of 0.008~0.065mg·mL-1. The average recovery of rutin was 98.58%, RSD=0.34%. Conclusion: This quality standard was capable of effectively controlling the quality of Sambucus chinensis Lindl.granules. The method is simple quick accurate and the result of determination is good.
Keywords:Sambucus chinensis Lindl. granules    Quality standard    Flavonoids    TLC    Determining content
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