| 葛黄丸的定性定量方法研究 |
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| 引用本文： | 刘晋华 屈梅芳 蔡大伟. 葛黄丸的定性定量方法研究[J]. 中国药业, 2005, 14(10): 31-32 |
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| 作者姓名： | 刘晋华 屈梅芳 蔡大伟 |
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| 作者单位： | 中国人民解放军第二五一医院，中国人民解放军第二五一医院，中国人民解放军第二五一医院 河北 张家口 075000，河北 张家口 075000，河北 张家口 075000 |
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| 摘 要： | 目的:探讨葛黄丸的定性定量方法.方法:采用薄层色谱法对处方中的葛根、黄芩、苦丁茶、钩藤进行定性鉴别;采用高效液相色谱法对制剂中葛根所含葛根素的含量进行测定.结果:葛根素线性范围是0.100 6～0.503 0μg,平均加样回收率为99.17%,RSD为1.6%(n=6),葛黄丸中葛根素平均含量为4.1 mg/g.结论:该方法快速、简便、回收率高,结果准确、可靠.
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| 关 键 词： | 葛黄丸 薄层色谱法 高效液相色谱法 葛根 葛根素 |
| 文章编号： | 1006-4931（2005）10-0031-02 |
| 收稿时间： | 2004-11-08 |
| 修稿时间： | 2005-02-16 |
Study on Methods of Qualitative and Quantitative Analysis for Gehuang Pills |
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| Liu Jinhua, Qu Meifang, Cai Dawei. Study on Methods of Qualitative and Quantitative Analysis for Gehuang Pills[J]. China Pharmaceuticals, 2005, 14(10): 31-32 |
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| Authors: | Liu Jinhua Qu Meifang Cai Dawei |
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| Abstract: | Objective: To study the method for qualitative and quantitative analysis of Gehuang pills. Methods: Radix Puerariae, Radix Scutellariae, Ilex kudingcha,Ramulus Uncariae cum Vncis were identified by TLC, and the content of puerarin in Radix Puerariae was determined by HPLC. Results: The method showed a good linear relationship. The average recovery was 99. 17% with RSD = 1. 6% ( n =6); the average content of Puerarin in Gehuang pills was 4. 1 mg/g. Conclusion: This method is rapid, simple and results are satisfactory. |
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| Keywords: | Gehuang pills TLC HPLC Radix Puerariae Puerarin |
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