| 肿节风中异秦皮啶含量的HPLC法测定 |
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| 引用本文： | 周国平,刘红宇,王汉章,匡佩琳. 肿节风中异秦皮啶含量的HPLC法测定[J]. 中国中药杂志, 1999, 24(8): 481-482 |
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| 作者姓名： | 周国平 刘红宇 王汉章 匡佩琳 |
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| 作者单位： | 江西省药品检验所 南昌 330046 |
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| 摘 要： | 目的：建立肿节风中主要有效成分异秦皮啶的含量测定方法。方法：采用μＢｏｎｄａｐａｋＣ１８柱，乙腈０．１％磷酸（２０∶８０）为流动相，检测波长３４４ｎｍ。结果：平均回收率为９８．１％，ＲＳＤ为１．９％（ｎ＝５）。结论：提供了对肿节风质量控制的方法。
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| 关 键 词： | 肿节风 异秦皮啶 HPLC |
| 收稿时间： | 1998-01-06 |
Determination of Isofraxidin in Sarcandra glabra (Thunb.) Nakai by HPLC |
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| Zhou Guoping Liu Hongyu;Wang Hanzhang ; Kuang Peilin. Determination of Isofraxidin in Sarcandra glabra (Thunb.) Nakai by HPLC[J]. China Journal of Chinese Materia Medica, 1999, 24(8): 481-482 |
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| Authors: | Zhou Guoping Liu Hongyu Wang Hanzhang Kuang Peilin |
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| Affiliation: | Institute for Drug Control of Jiangxi Province, Nangchang 330046. |
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| Abstract: | OBJECTIVE: To establish a method for the determination of isofraxidin in Sarcandra glabra. METHOD: Using HPLC with mu-Bondapak C18 column, acetonitrile -0.1% phosphoric acid solution(20:80) as mobile phase and detection wavelength at 344 nm. RESULT: The recovery and RSD were 98.1% and 1.9% (n = 5) respectively. CONCLUSION: This method is rapid, simple and accurate, thus may be used for the quality control of this drug. |
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| Keywords: | Sarcandra glabra isofraxidin HPLC |
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