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枳实饮片中3类化学成分含量测定
引用本文:刘振丽,宋志前,张玲,李林福,王跃生.枳实饮片中3类化学成分含量测定[J].中国中药杂志,2006,31(17):1425-1427.
作者姓名:刘振丽  宋志前  张玲  李林福  王跃生
作者单位:1. 中国中医科学院,基础理论研究所,北京,100700
2. 中国中医科学院,中药研究所,北京,100700
摘    要:目的:测定枳实饮片中3类成分含量。方法: HPLC测定黄酮类成分橙皮苷和柚皮苷含量、生物碱类辛弗林含量,药典法测定挥发油含量。结果: 10个批次的饮片中橙皮苷含量为1.25%~16.6%,柚皮苷含量为0%~13.9%,相差很大。其中有3个批次的饮片中不含有柚皮苷,而橙皮苷含量却很高。柚皮苷与橙皮苷的含量之和相差不大,为10.8%~16.6%;辛弗林含量为0.058 5%~0.676%;挥发油含量为0.1%~2.2%,差异较大。结论:枳实饮片3类化学成分含量差别很大。

关 键 词:枳实  橙皮苷  柚皮苷  辛弗林  挥发油
文章编号:1001-5302(2006)17-1425-03
收稿时间:2005-06-27
修稿时间:2005-06-27

Determination of three chemical components in Fructus aurantii immaturus
LIU Zhen-li ;SONG Zhi-qian ;ZHANG Ling ;LI Lin-fu ;WANG Yue-sheng.Determination of three chemical components in Fructus aurantii immaturus[J].China Journal of Chinese Materia Medica,2006,31(17):1425-1427.
Authors:LIU Zhen-li ;SONG Zhi-qian ;ZHANG Ling ;LI Lin-fu ;WANG Yue-sheng
Institution:1. Institute of Basic Theory of Chinese Medicine, China Academy of Traditional Chinese Medicine, Beijing 100700, China; 2. Institute of Chinese Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China
Abstract:Objective: To determine the contents of 3 kinds of components in Fructus aurantii immaturus. Method: HPLC analysis was performed to detect the contents of hesperidin, naringin and synephrine. The content of volatile oil was detected determined following the method of Chinese pharmacopoeia. Result: The contents of hesperidin, naringin, synephrine and volatile oil in ten samples are from 1.25% to 16.6%, 0% to 13.9%, 0.058 5% to 0.676% and 0.1% to 2.2% , respectively. Conclusion: The contentre are significant differences of among chemical components in from different samples of Fructus aurantii immaturus are greats.
Keywords:Fructus aurantii immaturus  hesperidin  naringin  synephrine  volatile oil
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