| 玻璃输液瓶中砷浸出量的原子荧光光谱法测定 |
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| 引用本文： | 周红娇. 玻璃输液瓶中砷浸出量的原子荧光光谱法测定[J]. 中国医药导报, 2011, 8(17): 146-147 |
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| 作者姓名： | 周红娇 |
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| 作者单位： | 云南省医疗器械检验所,云南昆明,650034 |
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| 摘 要： | 目的：建立氢化物发生-原子荧光光谱法HG-AFS测定药包材中玻璃输液瓶的砷浸出量方法。方法：样品液直接用原子荧光光谱法测定,并对HG-AFS工作参数及条件进行优化和选择。结果：标准曲线线性良好,相关系数r=0.999 4,检出限0.064μg/L,回收率为97.80%,RSD为2.04%。结论：原子荧光光谱法简便、快速准确、灵敏度高。
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| 关 键 词： | 药包材 玻璃输液瓶 砷浸出量测定 氢化物发生一原子荧光光谱法 |
Determination of arsenic releases from glass infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometry |
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| ZHOU Hongjiao. Determination of arsenic releases from glass infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometry[J]. China Medical Herald, 2011, 8(17): 146-147 |
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| Authors: | ZHOU Hongjiao |
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| Affiliation: | ZHOU Hongjiao Yunnan Province Institute of Testing on Medical Appliance,Kunming 650034,China |
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| Abstract: | Objective： To establish a method for determination of arsenic release from Glass Infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometer（HG-AFS）.Methods： Sample solutions were directly determined by HG-AFS.Operation parameters of HG-AFS and condition were optimized and selected.Results： A good linearity was obtained（r=0.999 4）.The detection limit was 0.064 μg/L.The recovery was 97.80%.RSD was 2.04%.Conclusion： The HG-AFS method is simple and fast with high sensitivity. |
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| Keywords: | Drug packaging materials Glass infusion bottles Release of arsenic HG-AFS |
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