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HPLC法测定复方益肾胶囊中淫羊藿苷的含量
引用本文:肖佳尚.HPLC法测定复方益肾胶囊中淫羊藿苷的含量[J].中国医药导报,2011,8(16):68-70.
作者姓名:肖佳尚
作者单位:广州市黄埔区食品药品检验所,广东广州,510700
摘    要:目的:建立复方益肾胶囊中淫羊藿苷的含量测定方法,为复方益肾胶囊质量标准研究提供依据。方法:采用高效液相色谱法测定中药复方益肾胶囊中淫羊藿苷的含量。以Diamnosil C18(4.6 mm×250 mm,5μm)为色谱柱,乙腈-0.1%磷酸(25∶75)为流动相;检测波长为270 nm。结果:此方法线性良好,平均加样回收率为98.7%。结论:本方法精密度高,分离度良好,可用于中药复方益肾胶囊中淫羊藿苷的含量测定。

关 键 词:复方益肾胶囊  淫羊藿苷  高效液相色谱  含量测定

Determination of icariin in Fufang Yishen Capsule by HPLC
XIAO jiashang.Determination of icariin in Fufang Yishen Capsule by HPLC[J].China Medical Herald,2011,8(16):68-70.
Authors:XIAO jiashang
Institution:XIAO Jiashang Institute for Food and Drug Control of Huangpu District in Guangzhou City,Guangdong Province,Guangzhou 510700,China
Abstract:Objective: To establish a HPLC method for the content determination of icariin in Fufang Yishen Capsule.Methods: HPLC method was used to determine the content determination of icariin in Fufang Yishen Capsule with Diamonsil C18(4.6 mm×250 mm,5 μm) as column,mobile phase consisted of Acetonitrile-0.1% potassium(25∶75),UV was 270 nm.Results: Linearity of this method was well with the average recoveries was 98.7%.Conclusion: This method is accurate,reliable and repeatable;it can be used to control the standard of Fufang Yishen Capsule.
Keywords:Fufang Yishen Capsule  Icariin  HPLC  Determination  
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