| 百桔止咳颗粒的质量标准研究 |
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| 引用本文： | 李培毅,裴小静,冯玛莉,牛艳艳,贾力莉.百桔止咳颗粒的质量标准研究[J].山西中医学院学报,2006,7(1):47-49. |
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| 作者姓名： | 李培毅 裴小静 冯玛莉 牛艳艳 贾力莉 |
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| 作者单位： | 山西省中医药研究院,山西,太原,030012 |
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| 摘 要： | 目的:研究制定百桔止咳颗粒的质量控制指标。方法:采用薄层色谱法对百桔止咳颗粒中的青蒿、桔梗、甘草等药味进行了定性鉴别;采用高效液相色谱法对制剂中的橙皮苷进行了含量测定。结果:青蒿、桔梗、甘草等药味的薄层色谱清晰,无干扰,重现性良好;橙皮苷在0.041μg￣0.203μg范围内呈良好的线性关系,回收率达到100.40%,RSD=2.37%。结论:方法简便,专属性强,可作为该制剂的质量控制指标。
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| 关 键 词： | 百桔止咳颗粒 薄层色谱 高效液相色谱 橙皮苷 |
| 文章编号： | 1671-0258(2006)01-0047-03 |
| 收稿时间： | 10 12 2005 12:00AM |
| 修稿时间： | 11 20 2005 12:00AM |
Quality Standards of Baijie Zhike Granule |
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| Li Peiyi,Pei Xiaojing,Feng Mali,Niu Yanyan,Jia Lili.Quality Standards of Baijie Zhike Granule[J].Journal of Shanxi College of Traditional Chinese Medicine,2006,7(1):47-49. |
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| Authors: | Li Peiyi Pei Xiaojing Feng Mali Niu Yanyan Jia Lili |
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| Institution: | Shanxi Academy of Traditional Chinese Medicine and Materia Medica, Taiyuan Shanxi 030012 |
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| Abstract: | Objective:To study the quality standards of Baijie Zhike Granule. Methods:Herba Artemisiae Annu-ae, Radix Platycodi, Radix Glycyrrhizae were identified by TLC, and Hesperidin was determined by HPLC. Results:TLC spots developed were fairly clear, and the blank test showed no interference. Hesperidin showed a good linear relationship in the concentration range of 0.041 μg~0.203 μg. The average recovery rate was up to 100.40 %, RSD was 2.37%. Conclusions:These methods are simple with strong specificity and good reproducibility, and can be used as the quality control of this preparation. |
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| Keywords: | Baijie Zhike granule TLC HPLC Hesperidin |
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