| 紫苏梗的化学成分研究 |
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| 引用本文： | 宋明明,尚志春,付晓雪,于大勇,王永奇,史丽颖.紫苏梗的化学成分研究[J].中国药房,2014(31):2947-2948. |
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| 作者姓名： | 宋明明 尚志春 付晓雪 于大勇 王永奇 史丽颖 |
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| 作者单位： | 大连大学药物研究所,辽宁大连116622 |
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| 摘 要： | 目的:研究紫苏梗的化学成分。方法:采用硅胶柱色谱、Sephadex LH-20柱色谱等对紫苏梗95%乙醇提取物的乙酸乙酯部位进行分离纯化,根据波谱学数据和理化性质进行结构鉴定。结果:共分离并鉴定了6个化合物,分别为:胡萝卜苷(1)、齐墩果酸(2)、常春藤皂苷元(3)、芹菜素(4)、2,6-二甲氧基苯醌(5)、肌醇(6)。结论:化合物1、3、4、5和6均为首次从紫苏梗中分离得到。
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| 关 键 词： | 紫苏梗 化学成分 提取分离 结构鉴定 |
Study on the Chemical Constituents in the Stem of Perillafrutescens |
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| SONG Ming-ming,SHANG Zhi-chun,FU Xiao-xue,YU Da-yong,WANG Yong-qi,SHI Li-ying.Study on the Chemical Constituents in the Stem of Perillafrutescens[J].China Pharmacy,2014(31):2947-2948. |
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| Authors: | SONG Ming-ming SHANG Zhi-chun FU Xiao-xue YU Da-yong WANG Yong-qi SHI Li-ying |
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| Institution: | (Institute of Ma- teria Medica, Dalian University, Liaoning Dalian 116622, China) |
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| Abstract: | OBJECTIVE： To study the chemical constituents of the stem of Perilla frutescens. METHODS： Silica gel column chromatography and Sephadex LH-20 column chromatography were used for the separation and purification from acetic ether part of 95 % ethanol extract from P. frutescens; and the structure of chemical constituents were identified by spectroscopy data and physi- cochemical characters. RESULTS： 6 compounds were isolated and identified, as daucosterol（1）, oleanolic acid（2）, apigenin （3）, hederagenin （4）, 2, 6-dimethoxy benzene quinone（5）, inositol （6）. CONCLUSIONS： Compoundsl, 3, 4, 5 and 6 are obtained from the stem of P. frutescens for the first time. |
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| Keywords: | Perillafrutescens Chemical constituents Extraction and isolation Structural identification |
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