| HPLC测定前列舒乐片中淫羊藿苷的含量 |
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| 引用本文： | 肖俭,赵子剑. HPLC测定前列舒乐片中淫羊藿苷的含量[J]. 光明中医, 2010, 25(6): 952-954. DOI: 10.3969/j.issn.1003-8914.2010.06.0024 |
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| 作者姓名： | 肖俭 赵子剑 |
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| 作者单位： | 湖南洞口县人民医院,洞口,422300;湖南省怀化学院,怀化,418008 |
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| 摘 要： | 目的建立前列舒乐片中淫羊藿苷的含量测定方法。方法采用高效液相色谱法测定,用C18柱(150mm×4.6mm,5μm),以乙腈∶水(28∶72)为流动相,检测波长270nm。结果淫羊藿苷的线性范围为0.25～1.50μg;相关系数r=0.9999,平均回收率为98.62%,RSD=0.52%(n=10);结论所用方法测定样品灵敏度高,重复性好,能有效地控制前列舒乐片的质量。
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| 关 键 词： | 前列舒乐片 淫羊藿苷 HPLC |
Determination of Icraiin in Qianlie Shule Pian by HPLC |
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| Xiao Jian,Zhao Zijian. Determination of Icraiin in Qianlie Shule Pian by HPLC[J]. Journal of Traditional Chinese Medicine, 2010, 25(6): 952-954. DOI: 10.3969/j.issn.1003-8914.2010.06.0024 |
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| Authors: | Xiao Jian Zhao Zijian |
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| Affiliation: | 1.People＇ s Hospital of Dongkou County Dongkou, Hunan 422300 ;2. Huaihua University, Huaihua, Hunan 418008) |
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| Abstract: | Objective：To establish method for the determination of Icraiin in Qianlie Shule Pian; Methods：The separation was carried out on C18 column（ 150mm × 4. 6mm, 5um）;The mobile phase was composed of CH3CN-H2O （28： 72）, Detection wavelength was 270nm. Results：The linear range of [craiin was 0. 25 - 1. 50ug （r = 0. 9999） ; Average recovery was 98.26% （ RSD = 0. 52% ; n = 10）. Conclusion：This method was high sensitivity, good reproducibility and suitable for the quality control of this preparation. |
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| Keywords: | HPLC |
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