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| 不同商品规格川贝母总生物碱含量测定的方法研究 | |
| 引用本文： | 王纯玉,何祖新,吴玉良. 不同商品规格川贝母总生物碱含量测定的方法研究[J]. 中国药业, 2013, 22(15): 31-33 |
| 作者姓名： | 王纯玉 何祖新 吴玉良 |
| 作者单位： | 1. 四川省攀枝花市中西医结合医院,四川攀枝花,617000 2. 成都中医药大学,四川成都,611137 3. 四川康定金珠制药有限责任公司,四川康定,626100 |
| 摘 要： | 目的 建立酸性染色法用于测定川贝母中总生物碱的含量.方法 采用三氯甲烷-甲醇(4∶1)混合溶液提取川贝母总生物碱；采用酸性染料染色法,以西贝母碱为指标成分,测定总生物碱的含量.结果 4个规格川贝母样品中总生物碱含量均符合2010年版《中国药典(一部)》的规定.结论 该方法不需要复杂仪器、操作简便,可作为川贝母的质量检测方法. |
| 关 键 词： | 川贝母 酸性染料比色法 总生物碱 含量测定 |
Method Study of Determination on Total Alkaloid Content in Different Commercial Specifications of Fritillaria Cirrhosa |
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| Wang Chunyu , He Zuxin , Wu Yuliang. Method Study of Determination on Total Alkaloid Content in Different Commercial Specifications of Fritillaria Cirrhosa[J]. China Pharmaceuticals, 2013, 22(15): 31-33 | |
| Authors: | Wang Chunyu He Zuxin Wu Yuliang |
| Affiliation: | 1. Panzhihua Municipal Hospital of Integrated Chinese and Western Medicine, Panzhihua, Sichuan, China 617000; 2. Chengdu University of Traditional Chinese Medicine, Chengdu, Sichuan, China 611137; 3. Kangding Jinzhu Pharmaceutical Co., Ltd., Kangding, Sichuan, China 626100) |
| Abstract: | Objective To establish the acid staining method for the determination of total alkaloid content in Fritillaria Cirrhosa. Methods The mixed solution of trichloromethane-methanol （4 ： 1 ） was adopted to extract total alkaloids in Fritillaria Cirrhosa; the acid dye staining method was used to determine the content of total alkaloids with imperialine as the index components. Methods The content of total alkaloids in 4 specifications of samples of Fritillaria Cirrhosa all were in line with the stipulation of the Chinese Phar-macopoeia （edtion 2010, Part 1）. Conclusion This method does not require the sophisticated instruments, is easy and simple to operate and can be used as the quality testing method of Fritillaria Cirrhosa. |
| Keywords: | Fritillaria cirrhosa acid dyes colorimetry total alkaloid content determination |
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