| 毛细管柱气相色谱法测定食品中的甜蜜素 |
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| 引用本文： | 周华. 毛细管柱气相色谱法测定食品中的甜蜜素[J]. 中国卫生检验杂志, 2007, 17(4): 649-649,686 |
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| 作者姓名： | 周华 |
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| 作者单位： | 浙江省衢州市疾病预防控制中心,浙江衢州,324000 |
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| 摘 要： | 目的：建立毛细管柱气相色谱法测定食品中的甜蜜素的方法。方法：采用适当的样品处理方法，应用弱极性的HP-1毛细管柱取代填充柱检测食品样品中的甜蜜素。结果：在最佳分析条件下，样品中的甜蜜素经酯化后在0.50～3．0mg/ml范围内有良好的线性（r=0．9998），回收率为94．1％～97．6％，相对标准偏差3．0％～4.9％。结论：相对于国家标准方法推荐的填充柱，毛细管柱的柱效高，通用性好，结果更易重复，是食品中甜蜜素检测的另一选择。
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| 关 键 词： | 毛细管柱气相色谱法 食品 甜蜜素 |
| 文章编号： | 1004-8685（2007）04-0649-02 |
| 收稿时间： | 2007-01-15 |
| 修稿时间： | 2007-01-15 |
Determination of sodium cyclamate in food by capillary gas chromatography |
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| Zhou Hua. Determination of sodium cyclamate in food by capillary gas chromatography[J]. Chinses Journal of Health Laboratory Technology, 2007, 17(4): 649-649,686 |
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| Authors: | Zhou Hua |
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| Affiliation: | Quzhou Center for Disease Control and Prevention, Quzhou 324000, China |
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| Abstract: | Objective:To establish a method for the determination of sodium cyclamate in food by capillary gas chromatography.Methods:Using proper sample treatment method,applying non-polar capillary column(HP-1) to replace packed column for the determination of sodium cyclamate in food.Results:Under the best condition,calibration curves showed good linear relationship within the range of 0.50~3.00 mg/ml(r=0.9998) after the reaction of esterification occur.The method recovery was 94.1%~97.6% and the relative standard deviation was 3.0%~4.9%.Conclusion:Capillary column has better column efficiency,commonality and repeatability relative to packed column that is recommended by national standard method.It is another choice for the determination of sodium cyclamate in food. |
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| Keywords: | Capillary gas chromatography Food Sodium cyclamate |
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