| HPLC-UV法测定箭羽糖康片中芒果苷的含量 |
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| 引用本文： | 白林,郝爱真,金道山,徐元杰,张慧. HPLC-UV法测定箭羽糖康片中芒果苷的含量[J]. 军医进修学院学报, 2010, 31(10): 1007-1008,1013 |
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| 作者姓名： | 白林 郝爱真 金道山 徐元杰 张慧 |
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| 作者单位： | [1]解放军总医院药品保障中心药检室 [2]解放军总医院中医科,北京100853 [3]蚌埠医学院,蚌埠233003 |
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| 摘 要： | 目的建立箭羽糖康片质量控制方法。方法采用HPLC-UV法测定箭羽糖康片中芒果苷的含量,流动相为乙腈-水（12∶88）,用0.85%的磷酸调pH至2.85,流速0.8ml/min,检测波长258nm。柱温30℃。结果芒果苷在3.9-390μg/ml范围内呈现良好的线性关系（r=0.9999）。样品平均回收率为97.718%,RSD为0.92%。结论建立HPLC-UV法测定箭羽糖康片中的芒果苷含量,方法简便准确,灵敏度高,能有效地控制制剂质量。
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| 关 键 词： | 箭羽糖康片 HPLC—UV 芒果苷 |
Measurement of mangiferin level in Jianyu tangkang tablets with HPLC-UV |
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| BAI Lin,HAO Ai-zhen,JIN Dao-shan,XU Yuan-jie,ZHANG Hui. Measurement of mangiferin level in Jianyu tangkang tablets with HPLC-UV[J]. Academic Journal of Pla Postgraduate Medical School, 2010, 31(10): 1007-1008,1013 |
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| Authors: | BAI Lin HAO Ai-zhen JIN Dao-shan XU Yuan-jie ZHANG Hui |
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| Affiliation: | 1.Department of Drug Analysis, Medicine Supply Center, Chinese PLA General Hospital, Beijing 100853, China; 2.Department of Traditional Chinese Medicine, Chinese PLA General Hospital, Beijing 100853, China;3.Bengbu Medical College, Bengbu 233003,Anhui Province, China) |
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| Abstract: | Objective To establish the quality control method of Jianyu tangkang tablets. Methods HPLC-UV was used to measure the mangiferin level in Jianyu tangkang tablets on a C18-ODS column （250mm×4.6mm, 5μm） at the mobile phase of acetonitrile and water （12∶88, pH=2.85）, with a detection wavelength of 258nm, a flow rate of 0.8ml/min, and a column temperature of 30℃. Results A good linear relationship was observed when the mangiferin level was 3.9-390μg/ml（r=0.999 9）. The average recovery rate of samples was 97.718%（RSD=0.92%）. Conclusion HPLC-UV is a simple, rapid, accurate, and sensitive method, which can effectively control the quality of Jianyu tangkang tablets. |
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| Keywords: | Jian Yu Tang Kang Tablet HPLC-UV Mangiferin |
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